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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 13
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Original Articles

CONTINUOUS OPTICAL RESOLUTION OF (p-IODOPHENYL)GLYCINOL

Pages 2061-2066 | Received 24 Jul 2001, Published online: 16 Aug 2006
 

ABSTRACT

Enantiomeric enrichment of racemic (p-iodophenyl)glycinol was achieved with various optically active organic acids. The scalemic mixtures were further resolved by entrainment with racemic crystals of the starting material. The pure enantiomers were recovered from the mother liquor; the crystalline—almost racemic—base was recycled.

Acknowledgments

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