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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 18
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Original Articles

DEPROTECTION OF 1,1-DIACETATES WITH [NO+ ⋅ CROWN ⋅ H(NO3)2−]

Mohammad Ali Zolfigol Chemistry Department, College of Science, Bu-Ali Sina University, Hamadan, 65174, IranCorrespondence[email protected]
,
Mohammad Hassan Zebarjadian Chemistry Department, College of Science, Bu-Ali Sina University, Hamadan, 65174, Iran
,
Iraj Mohammadpoor-Baltork Chemistry Department, College of Science, Isfahan University, Isfahan, I.R. Iran
&
Mojtaba Shamsipur Chemistry Department, College of Science, Razi University, Kermanshah, Iran
Pages 2803-2808 | Received 26 Jul 2001, Published online: 18 Oct 2011
 
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ABSTRACT

An ionic complex has been obtained from N2O4 in the presence of the macrocyclic polyether 18-crown-6. This crystalline compound was used as an effective deprotecting agent for the conversion of 1,1-diacetates to their corresponding aldehydes at room temperature with quantitative yields.

ACKNOWLEDGMENT

The financial support for this work by the research affairs of Bu-Ali Sina University, Hamadan, Iran is acknowledged.

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