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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 20
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Original Articles

PHASE TRANSFER CATALYZED SYNTHESIS OF 1-ARYLOXYACETYL- 4-(2-METHYLPHENYLOXYACETYL)-THIOSEMICARBAZIDES UNDER MICROWAVE IRRADIATION

Guolin Zhang Department of Chemistry, Lanzhou Medical College, Lanzhou, Gansu, 730000, P.R. China
,
Zheng Li College of Chemistry and Chemical Engineering, Northwest Normal University, Lanzhou, Gansu, 730070, P.R. China
&
Xicun Wang College of Chemistry and Chemical Engineering, Northwest Normal University, Lanzhou, Gansu, 730070, P.R. ChinaCorrespondence[email protected]
Pages 3107-3112 | Received 10 Jul 2001, Published online: 16 Aug 2006
 
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ABSTRACT

The 1-aryloxyacetyl-4-(2-methylphenyloxyacetyl)-thiosemicarbazides (3a–l) are synthesized via reaction of 2-methylphenyloxyacetyl chloride with ammonium thiocyanate and aryloxyacetic acid hydrazides (2a–l) under phase transfer catalysis and microwave irradiation in excellent yield.

ACKNOWLEDGMENTS

The authors are grateful for financial support for this work from Scientific and Technological Innovation Engineering of Northwest Normal University, Natural Science Foundation of Gansu Province, and Youth Foundation of Northwest Normal University.

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