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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 23
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Original Articles

A CONVENIENT SYNTHESIS OF OXETENE VIA [2+2]CYCLOADDITION REACTION UNDER MICROWAVE IRRADIATION

M. Longchar Organic Chemistry Division, Regional Research Laboratory, Jorhat, 785 006, India
,
U. Bora Organic Chemistry Division, Regional Research Laboratory, Jorhat, 785 006, India
,
R. C. Boruah Organic Chemistry Division, Regional Research Laboratory, Jorhat, 785 006, IndiaCorrespondence[email protected]
&
J. S. Sandhu Organic Chemistry Division, Regional Research Laboratory, Jorhat, 785 006, India
Pages 3611-3616 | Received 22 Nov 2001, Published online: 16 Aug 2006
 
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ABSTRACT

A facile and fast preparation of oxetene has been reported by a microwave mediated [2+2]cycloaddition reaction of steroidal formyl enamides and alkynes in a solventless condition.

ACKNOWLEDGMENTS

We thank the Department of Science and Technology (DST), New Delhi for financial support of this work. One of us (ML) thanks University Grant Commission (UGC), New Delhi for award of a Teacher Fellowship.

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