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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 33, 2003 - Issue 4
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Original Articles

Microwave Promoted Rapid Oxidation of Alcohols Using Cobalt Nitrate Hexahydrate Supported on Silica Gel Under Solvent Free Conditions

A. R. Kiasat Chemistry Department, College of Science, Shahid Chamran University, Ahvaz, IranCorrespondence[email protected]
,
F. Kazemi Chemistry Department, College of Science, Shahid Chamran University, Ahvaz, IranCorrespondence[email protected]
&
M. Rafati Ghachsaran Islamic Azad University, Ghachsaran, Iran
Pages 601-605 | Received 03 Dec 2001, Published online: 16 Aug 2006
 
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Abstract

A new method for oxidation of alcohols into the corresponding carbonyl compounds by treatment with cobalt nitrate hexahydrate adsorbed on silica gel is described. This reagent can be used as an effective and mild oxidizing agent for this transformation under microwave irradiation in dry media, and high yields. Over oxidation of the formed aldehydes was not observed.

Acknowledgment

We would like to acknowledge the partial support of this work by Ghachsaran Islamic Azad University Research Council.

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