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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 33, 2003 - Issue 5
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Original Articles

Soluble Polymer-Supported Synthesis of Tertiary Amines

Zuxing Chen Faculty of Chemistry and Material Science, Hubei University, Wuhan, Hubei, P.R. ChinaCorrespondence[email protected]
,
Guichun Yang Faculty of Chemistry and Material Science, Hubei University, Wuhan, Hubei, P.R. China
&
Zhaojun Zhang Faculty of Chemistry and Material Science, Hubei University, Wuhan, Hubei, P.R. China
Pages 729-734 | Received 13 Nov 2001, Published online: 17 Aug 2006
 
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Abstract

The synthesis of tertiary amines on a modified soluble polymer, poly(ethylene glycol) (PEG), is described. The PEG-bound quaternary intermediates were assembled via Michael addition reaction, followed by alkylation. Cleavage from the soluble polymer support was induced by insoluble weak basic resin, to afford the target tertiary amines in excellent purity.

Acknowledgment

Financial supports were provided by Education Department of Hubei Province and Hubei University.

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