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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 33, 2003 - Issue 5
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Original Articles

Synthesis of Unsymmetrical Divinylbenzenes by Palladium Catalyzed Sequential Heck Reactions Starting from Carboxybenzenediazonium Salts

Chao Wang Department of Chemistry, Nanjing University, Nanjing, China
,
Lu-Shi Tan Department of Chemistry, Nanjing University, Nanjing, China
,
Jin-Ping He Department of Chemistry, Nanjing University, Nanjing, China
,
Hong-Wen Hu Department of Chemistry, Nanjing University, Nanjing, China
&
Jian-Hua Xu Department of Chemistry, Nanjing University, Nanjing, ChinaCorrespondence[email protected]
Pages 773-782 | Received 25 Dec 2001, Published online: 17 Aug 2006
 
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Abstract

Six p-, m- and o-unsymmetrical divinylbenzenes 5a, 5b, 6a, 6b, 6c and 7a are synthesized from p-, m- and o- carboxybenzenediazonium tetrafluoroborates via sequential Heck reactions in good overall yield.

Acknowledgment

This work was supported by the National Natural Science Foundation of China (Project 20072017).

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