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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 33, 2003 - Issue 5
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Original Articles

Synthesis of Ethyl α-Cyanocinnamates Catalyzed by Al2O3–OK Solid Base

Tong-Shou Jin Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, P.R. ChinaCorrespondence[email protected]
,
Jun-Jie Guo Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, P.R. China
,
Hui-Min Liu Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, P.R. China
&
Tong-Shuang Li Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, P.R. China
Pages 783-788 | Received 20 Nov 2001, Published online: 17 Aug 2006
 
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Abstract

Condensation of ethyl cyanoacetate with aromatic aldehydes catalyzed by Al2O3–OK solid base in ethanol results ethyl α-cyanocinnamates in 80–99% yields.

Acknowledgments

The project was supported by National Natural Science Foundation of China (29872011 and 29572039), Educational Ministry of China, Educational Department of Hebei Province (990104), and Science and Technology Commission of Hebei Province.

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