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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 33, 2003 - Issue 6
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Original Articles

Synthesis of New Biosynthetically Important Diarylheptanoids and Their Oxa- and Fluoro- Analogues by Three Different Strategies

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Pages 1019-1045 | Received 25 Jan 2002, Published online: 17 Aug 2006
 

Abstract

Wittig, aldol and Wittig-Horner reactions have been used to synthesize new diarylheptanoids, which are putative intermediates in phenylphenalenone biosynthesis in plants. The Wittig-Horner approach was most suitable and gave significantly higher yields in comparison with other methods.

Acknowledgments

The authors thank Dr. Neil J. Oldham and Janine Rattke, Jena, for mass spectra. This investigation was supported financially by the Deutsche Forschungsgemeinschaft (Bonn) and the Fonds der Chemischen Industrie (Frankfurt/Main).

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