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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 33, 2003 - Issue 7
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Original Articles

A New Entry for the Preparation of Substituted Aromatic Carbonyl Compounds Mediated by Samarium(II) Iodide

Hidemi Yoda Department of Molecular Science, Faculty of Engineering, Shizuoka University, Johoku, Hamamatsu, JapanCorrespondence[email protected]
,
Naoki Kohata Department of Molecular Science, Faculty of Engineering, Shizuoka University, Johoku, Hamamatsu, Japan
&
Kunihiko Takabe Department of Molecular Science, Faculty of Engineering, Shizuoka University, Johoku, Hamamatsu, Japan
Pages 1087-1094 | Received 18 Feb 2002, Published online: 21 Aug 2006
 
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Abstract

A new route to substituted aromatic lactones and lactams via SmI2-promoted desulfurization is described. Direct replacement of the phenylthio substituent by hydroxyalkylated groups featuring the novel accessible process for the construction of continuous quaternary carbon centers could be accomplished when the same type of reactions was undertaken with carbonyl compounds in the presence of SmI2.

Acknowledgments

This work was partially supported by a Grant-in Aid (No. 13640530) from the Ministry of Education, Science, Sports and Culture of Japan.

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