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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 33, 2003 - Issue 12
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Original Articles

A Highly Efficient and Chemoselective Method for Acetalization of Carbonyl Compounds Catalyzed by Solid Superacid

Yan-Ran Ma Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, Hebei Province, P.R. China
,
Tong-Shou Jin Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, Hebei Province, P.R. ChinaCorrespondence[email protected]
,
Sheng-Xun Shi Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, Hebei Province, P.R. China
&
Tong-Shuang Li Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, Hebei Province, P.R. China
Pages 2103-2108 | Received 01 Oct 2002, Published online: 17 Aug 2006
 
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Abstract

Various types of aldehydes and ketones could be converted to their corresponding diethyl acetals with triethylorthoformate in the presence of solid superacid in good to excellent yield under mild reaction conditions.

Acknowledgments

The work was supported by NSFC (29872011 and 29572039), Education Ministry of China and Education Department of Hebei Province (990104) and Science and Technology Commission of Hebei Province.

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