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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 33, 2003 - Issue 15
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Original Articles

A Facile Synthesis of Substituted N-Benzoylthiourea

Xiaoyong Xu Institute of Pesticides and Pharmaceuticals, East China University of Science and Technology, Shanghai, China; Shanghai Key Lab of Chemical Biology, ECUST, China
,
Zhongli Institute of Pesticides and Pharmaceuticals, East China University of Science and Technology, Shanghai, China; Shanghai Key Lab of Chemical Biology, ECUST, China
,
Zhengyu Yang Institute of Pesticides and Pharmaceuticals, East China University of Science and Technology, Shanghai, China
,
Gang Chen Institute of Pesticides and Pharmaceuticals, East China University of Science and Technology, Shanghai, China; Shanghai Key Lab of Chemical Biology, ECUST, China
&
Xuhong Qian State Key Laboratory of Fine Chemicals, Dalian University of Technology, Dalian, ChinaCorrespondence[email protected] [email protected]
Pages 2585-2592 | Received 15 Oct 2002, Published online: 17 Aug 2006
 
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Abstract

One pot reaction of benzoyl isothiocyanate and Tris(hydroxy- methyl)aminomethane (Tris) at room temperature with polyethylene glycol-400 (PEG-400) as solid–liquid phase-transfer catalyst produced substituted N-benzoylthioureas with high yield. A reasonable pathway for their formation has been suggested.

Acknowledgment

This work was partly supported by National 863 High-tech Research Award, National Natural Science Foundation of China, The Ministry of Education and Science and Technology foundation of Shanghai.

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