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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 33, 2003 - Issue 18
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Original Articles

Alkylation of Dimethyl 1,3-Acetonedicarboxylate

Adrián Covarrubias-Zúñiga Instituto de Química, Universidad Nacional Autónoma de México, Ciudad Universitaria, Coyoacán, MéxicoCorrespondence[email protected]
,
Laura San Germán-Sanchez Instituto de Química, Universidad Nacional Autónoma de México, Ciudad Universitaria, Coyoacán, México
&
José G. Avila-Zárraga Facultad de Química, Universidad Nacional Autónoma de México, Ciudad Universitaria, Coyoacán, México
Pages 3165-3172 | Received 18 Dec 2002, Published online: 17 Aug 2006
 
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Abstract

A reliable, reproducible, general, and detailed procedure for the alkylation of dimethyl-1,3-acetonedicarboxylate is described.

Acknowledgments

This research was supported by a Grant-in Aid for Scientific Research No. 27610-E from CONACYT, México. The authors thank Professor J. Muchowski and Dr. N. Zúñiga for helpful discussions, We thank Messrs. R. Gaviño, R. Patiño, L. Velasco, and F. J. Pérez for running the spectra.

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