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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 2
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Original Articles

Pinacol-Pinacolone Rearrangement on FeCl3 Modified Montmorillonite K10

Ajit B. Shinde Organic Chemistry Research Laboratory, Institute of Chemical Technology, University of Mumbai, N. M. Parekh Road, Matunga, Mumbai, 400 019, India
,
Nilesh B. Shrigadi Organic Chemistry Research Laboratory, Institute of Chemical Technology, University of Mumbai, N. M. Parekh Road, Matunga, Mumbai, 400 019, India
,
Ramakrishna P. Bhat Organic Chemistry Research Laboratory, Institute of Chemical Technology, University of Mumbai, N. M. Parekh Road, Matunga, Mumbai, 400 019, India
&
Shriniwas D. Samant Organic Chemistry Research Laboratory, Institute of Chemical Technology, University of Mumbai, N. M. Parekh Road, Matunga, Mumbai, 400 019, IndiaCorrespondence[email protected]
Pages 309-314 | Received 18 Mar 2003, Published online: 18 Oct 2011
 
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Abstract

Pinacol-pinacolone rearrangement was investigated over Fe-modified montmorillonite K10 catalysts in liquid phase. Exceptional activity was found to be associated with FeCl3 impregnated on K10 through its acetonitrile solution. 100% conversion of benzopinacol was observed in 10 minutes. The catalysts are recyclable.

Acknowledgment

We are thankful to G. D. Gokhale Charitable Trust, Mumbai, for the financial support.

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