Abstract
A concise synthesis of 3‐dimethyl(phenyl)silyl‐5‐oxo‐hexanoic acid 1, the precursor for a solid supported β‐silylethanol anchoring group has been achieved from ethyl 2‐ethoxycarbonyl‐3‐dimethyl(phenyl)silyl‐2‐propenoate 2 featuring amino acid catalysed Michael addition of acetone as the key step.
Acknowledgment
We thank Shreenivas Shreenath and D. P. Mondal of IIT, Kharagpur, for some help.