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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 9
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Original Articles

A Facile Preparation of Organyltellurophosphates

Jiang‐Min Chen Department of Chemistry, Zhejiang University (Xixi Campus), Hangzhou, 310028, P.R. China; Department of Chemistry, Gannan Teachers' College, Ganzhou, P.R. China
&
Xian Huang Department of Chemistry, Zhejiang University (Xixi Campus), Hangzhou, 310028, P.R. China; Laboratory of Organometallic Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai, P.R. ChinaCorrespondence[email protected].
Pages 1745-1752 | Received 25 Aug 2003, Published online: 16 Aug 2006
 
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Abstract

Organyltellurophosphates can be synthesized smoothly via the free radical reaction of diorganyl phosphites with diorganyl ditellurides using (diacetoxyiodo)benzene and sodium azide in moderate to good yields.

Acknowledgments

We thank the National Natural Science Foundation of China for its financial support of the project 20272050.

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