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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 10
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Original Articles

Solvent‐Free Synthesis of 1,5‐Benzothiazepines and Benzodiazepines on Inorganic Supports

Mitsuo Kodomari Department of Applied Chemistry, Shibaura Institute of Technology, Shibaura, Minato‐ku, Tokyo, 108‐8548, JapanCorrespondence[email protected]
,
Tomohiro Noguchi Department of Applied Chemistry, Shibaura Institute of Technology, Shibaura, Minato‐ku, Tokyo, 108‐8548, Japan
&
Tadashi Aoyama Department of Materials and Applied Chemistry, Faculty of Science and Engineering, Nihon University, Chiyoda‐ku, Tokyo, Japan
Pages 1783-1790 | Received 11 Dec 2003, Published online: 20 Aug 2006
 
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Abstract

1,5‐Benzothiazepines and 1,5‐benzodiazepines have been synthesized in solvent‐free conditions from chalcones and o‐aminothiophenol or o‐phenylenediamine in the presence of inorganic support. Silica gel was found to be an effective support for the synthesis of 1,5‐benzothiazepines, whereas alumina was effective for the synthesis of 1,5‐benzodiazepines.

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