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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 16
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Original Articles

Synthesis of Diacetals from Aldehydes and Ketones with Pentaerythritol Catalyzed by Silica Sulfate Under Microwave Irradiation

Tong‐Shou Jin College of Chemistry and Environmental Science, Hebei University, No. 88 Hezuo Road, Baoding, 071002, Hebei Province, P.R. ChinaCorrespondence[email protected]
,
Huan‐Xin Wang College of Chemistry and Environmental Science, Hebei University, No. 88 Hezuo Road, Baoding, 071002, Hebei Province, P.R. China
,
Kai‐Fang Wang College of Chemistry and Environmental Science, Hebei University, No. 88 Hezuo Road, Baoding, 071002, Hebei Province, P.R. China; Slichem Liquid Crystal Co., Ltd., Shijiazhuang, P.R. China
&
Tong‐Shuang Li College of Chemistry and Environmental Science, Hebei University, No. 88 Hezuo Road, Baoding, 071002, Hebei Province, P.R. China
Pages 2993-2999 | Received 19 Jan 2004, Published online: 06 Jan 2011
 
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Abstract

The synthesis of diacetals from pentaerythritol with aldehydes and ketones is carried out under microwave irradiation in 80–98% yields with silica sulfate as catalyst.

Acknowledgment

The project was supported by NSF(29872011), Educational Ministry of China, Educational Department of Hebei Province (990104) and Science and Technology Commission of Hebei Province.

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