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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 18
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Original Articles

Novel Transformation of Methoxy Tetralones During Demethylation with Boron Trifluoride Etherate and Acetic Anhydride

Ajoy K. Banerjee Centro de Química, IVIC, Apartado 21827, Caracas, 1020‐A, VenezuelaCorrespondence[email protected]
,
Liadis Bedoya Centro de Química, IVIC, Apartado 21827, Caracas, 1020‐A, Venezuela
,
William J. Vera Centro de Química, IVIC, Apartado 21827, Caracas, 1020‐A, Venezuela
,
Carlos Melean Centro de Química, IVIC, Apartado 21827, Caracas, 1020‐A, Venezuela
,
Henry Mora Centro de Química, IVIC, Apartado 21827, Caracas, 1020‐A, Venezuela
,
Manuel S. Laya Centro de Química, IVIC, Apartado 21827, Caracas, 1020‐A, Venezuela
&
Miguel Alonso Química Ecológica, Universidad de Los Andes, Departamento de Química, Facultad de Ciencias, Mérida, Venezuela
 show all
Pages 3399-3408 | Received 02 Jun 2004, Published online: 10 Jan 2011
 
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Abstract

Tetralones 3 and 9 on treatment with a mixture of boron trifluoride etherate and acetic anhydride underwent molecular transformations yielding the fully aromatized products 6 and 10, respectively, Oxidation of dimethoxy tetralin 13 with chromic acid and acetic acid afforded 6‐methoxy‐α‐tetralone 12.

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