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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 20
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Original Articles

Stereoselective Synthesis of cis‐1‐Aryl‐2‐benzoyl‐3,3‐dicyanocyclopropanes in the Presence of KF·2H2O

Zhongjiao Ren Department of Chemistry, Shanghai University, Shanghai, 200436, P.R. ChinaCorrespondence[email protected]
,
Weiguo Cao Department of Chemistry, Shanghai University, Shanghai, 200436, P.R. China; State Key Laboratory of Organometallic Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai, 200032, P.R. China
,
Weiyu Ding Department of Chemistry, Shanghai University, Shanghai, 200436, P.R. China
,
Yu Wang Department of Chemistry, Shanghai University, Shanghai, 200436, P.R. China
&
Lilin Wang Department of Chemistry, Shanghai University, Shanghai, 200436, P.R. China
Pages 3785-3792 | Received 22 Apr 2004, Published online: 19 Apr 2010
 
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Abstract

KF · 2H2O was found to be a highly efficient base for synthesis of cis‐1,2‐cyclopropanes with arsonium salt and olefins. The advantages of the process are mild reaction condition, easy workup, excellent yields, and high stereoselectivity.

Acknowledgment

Thanks are due to the National Natural Science Foundation of China for financial support.

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