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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 22
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Original Articles

A Facile and Efficient Procedure for the Transdithioacetalization of 1,1‐Diacetates Using POCl3‐Montmorillonite as Catalyst

Tong‐Shou Jin Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, No. 88 Hezuo Road, Baoding, 071002, Hebei Province, P.R.ChinaCorrespondence[email protected]
,
Guang Sun Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, No. 88 Hezuo Road, Baoding, 071002, Hebei Province, P.R.China
,
Yan‐Wei Li Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, No. 88 Hezuo Road, Baoding, 071002, Hebei Province, P.R.China
&
Tong‐Shuang Li Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, No. 88 Hezuo Road, Baoding, 071002, Hebei Province, P.R.China
Pages 4105-4110 | Received 29 Jul 2004, Published online: 10 Jan 2011
 
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Abstract

A rapid and efficient method for the transdithioacetalization of 1,1‐diacetates with 1,2‐dithioglycol was described in good to excellent yield catalyzed by POCl3‐montmorillonite.

Acknowledgments

The project was supported by National Natural Science Foundation of China (29872011 and 29572039), Educational Ministry of China, Educational Department of Hebei Province (990104), Science and Technology Commission of Hebei Province.

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