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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 22
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Original Articles

Suzuki–Miyaura Reaction of Unactivated Aryl Chlorides Using Benzimidazol‐2‐Ylidene Ligands

İsmail Özdemir Department of Chemistry, Inönü University, 44069, Malatya, TürkiyeCorrespondence[email protected]
,
Yetkin Gök Department of Chemistry, Inönü University, 44069, Malatya, Türkiye
,
Nevin Gürbüz Department of Chemistry, Inönü University, 44069, Malatya, Türkiye
,
Engin Çetinkaya Department of Chemistry, Ege University, Bornova‐İzmir, Türkiye
&
Bekir Çetinkaya Department of Chemistry, Ege University, Bornova‐İzmir, Türkiye
Pages 4135-4144 | Received 11 May 2004, Published online: 10 Jan 2011
 
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Abstract

Four functionalized bis(benzimidazolium) salts (2a–d) have been prepared and characterized by conventional spectroscopic methods and elemental analyses. A highly effective, easy to handle, and environmentally bengin process for palladium‐mediated Suzuki cross‐coupling was developed. The in situ prepared three‐component system Pd(OAc)2/bis(benzimidazolium) bromides (2a–d) and Cs2CO3 catalyzes quantitatively the Suzuki cross‐coupling of deactivated aryl chloride in aqueous media.

Acknowledgments

We thank Technological and Scientific Research Council of Türkiye TÜBİTAK (TÜBITAK COST D17) and Inönü University Research Fund for financial support of this work.

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