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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 22
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Original Articles

Microwave‐Assisted NiCl2 Promoted Acylation of Alcohols

Violetta Constantinou‐Kokotou Chemical Laboratories, Agricultural University of Athens, Iera Odos, 75, Athens, 11855, GreeceCorrespondence[email protected]
&
Anna Peristeraki Chemical Laboratories, Agricultural University of Athens, Iera Odos, 75, Athens, 11855, Greece
Pages 4227-4232 | Received 30 Mar 2004, Published online: 10 Jan 2011
 
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Abstract

A microwave oven acylation of alcohols by carboxylic acid anhydrides has been developed. NiCl2 has been proven an efficient catalyst for the acylation of primary, secondary, and tertiary alcohols and phenols under microwave conditions.

Acknowledgment

The authors thank the Greek Ministry of Education and European Community for financial support in the frame of fellowships for research “Heraklitos”.

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