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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 35, 2005 - Issue 1
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Original Articles

Microwave‐promoted One‐Pot Three‐Component Reaction to [60]Fulleropyrrolidine Derivatives

Jianming Zhang Department of Chemistry, School of Science, Shanghai University, Shanghai, China
,
Wen Yang Department of Chemistry, School of Science, Shanghai University, Shanghai, China
,
Ping He Key Laboratory of Organofluorine Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Science, Shanghai, 200032, China
,
Shizheng Zhu Key Laboratory of Organofluorine Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Science, Shanghai, 200032, ChinaCorrespondence[email protected]
&
Sheng Wang Department of Chemistry, School of Science, Shanghai University, Shanghai, China
Pages 89-96 | Received 01 Jul 2004, Published online: 05 Aug 2006
 
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Abstract

Under microwave irradiation and solvent‐free condition, one‐pot three‐component reaction of C60, amino acid and aldehyde gave the corresponding [60]fulleropyrrolidine derivatives via dipolar [2 + 3] cycloaddition in moderate to good yields. Compared to the conventional thermal heating method, it provides a convenient and expeditious route to N‐unsubstituted fulleropyrrolidines.

Acknowledgments

The authors thank the National Natural Science Foundation of China (NNSFC) (No. 20372077) and Innovation Foundation of Chinese Academy of Sciences for financial support.

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