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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 35, 2005 - Issue 4
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Original Articles

Synthesis of 7‐Keto‐Gö6976 (ICP‐103)

Sudipta Roy Department of Chemistry, Dartmouth College, Hanover, USA
,
Alan Eastman Department of Pharmacology and Toxicology, Dartmouth Medical School, Hanover, USA
&
Gordon W. Gribble Department of Chemistry, Dartmouth College, Hanover, USACorrespondence[email protected]
Pages 595-601 | Received 04 Nov 2004, Published online: 12 Apr 2011
 
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Abstract

An efficient synthesis of 7‐keto‐Gö6976 (ICP‐103) (3) is described that employs palladium(II) triflate in the final oxidative cyclization step.

Acknowledgments

This investigation was supported in part by the donors of the Petroleum Research Fund (PRF), administered by the American Chemical Society, the National Institutes of Health (CA 82220), and Wyeth.

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