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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 35, 2005 - Issue 5
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Original Articles

Phase‐Transfer Catalyzed Pseudohalogenation of Phosphorochloridates

Enxue Shi Beijing Institute of Pharmaceutical Chemistry, Beijing, P. R ChinaCorrespondence[email protected]
&
Chengxin Pei Beijing Institute of Pharmaceutical Chemistry, Beijing, P. R China
Pages 669-673 | Received 20 Oct 2004, Published online: 20 Aug 2006
 
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Abstract

Pseudohalogenation of phosphorochloridates by sodium pseudohalides with different phase transfer catalysts and solvents was optimized. Dialkyl and diaryl phosphorazidates phosphorocyanidates, and phosphor(isothiocyanidate)s were prepared in good yields from phosphorochloridates under two kinds of mild phase‐transfer catalyzed conditions respectively.

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