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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 35, 2005 - Issue 6
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Original Articles

HIO3 in the Presence of Wet SiO2: A Mild and Efficient Reagent for Selective Oxidation of Sulfides to Sulfoxides under Solvent‐Free Conditions

M. M. Lakouraj Department of Chemistry, Faculty of Science, University of Mazandaran, Babolsar, IranCorrespondence[email protected]
,
M. Tajbakhsh Department of Chemistry, Faculty of Science, University of Mazandaran, Babolsar, Iran
,
F. Shirini Department of Chemistry, Guilan University, Rasht, Iran
&
M. V. Asady Tamami Department of Chemistry, Faculty of Science, University of Mazandaran, Babolsar, Iran
Pages 775-784 | Received 10 Jun 2004, Published online: 20 Aug 2006
 
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Abstract

In the presence of wet SiO2, HIO3 is highly efficient for the selective oxidation of sulfides to sulfoxides. It may be applied to any type of dialkyl and alkyl aryl sulfides. It develops under solvent‐free conditions, and gives high yield in the presence of different functional groups on the sulfide at room temperature.

Acknowledgment

We greatly acknowledge the research councils of Mazandran University for their financial support.

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