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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 35, 2005 - Issue 8
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Original Articles

Preparation of 1,5‐Fused Tetrazoles Under Solvent‐Free Conditions

Hossein Eshghi Department of Chemistry, Ferdowsi University of Mashhad, Mashhad, IranCorrespondence[email protected]
&
Asadollah Hassankhani Department of Chemistry, Sistan & Baluchestan University, Zahedan, Iran
Pages 1115-1120 | Received 21 Oct 2004, Published online: 16 Aug 2006
 
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Abstract

A facile and efficient procedure is developed for a one‐pot synthesis of fused 1,5‐disubstituted tetrazoles from cyclic ketones and sodium azide in the presence of aluminum chloride in solvent‐free media. Advantages of this method are chemoselectivity, with high yields in a simple operation, and short reaction time under solvent‐free conditions.

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