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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 35, 2005 - Issue 13
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Original Articles

Novel and Efficient Synthesis of Water‐Soluble [60]Fullerenol by Solvent‐Free Reaction

Sheng Wang Department of Chemistry, School of Science, Shanghai University, Shanghai, China
,
Ping He Key Laboratory of Organofluorine Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai, China
,
Jian‐Min Zhang Department of Chemistry, School of Science, Shanghai University, Shanghai, China
,
Hu Jiang Department of Chemistry, School of Science, Shanghai University, Shanghai, China
&
Shi‐Zheng Zhu Key Laboratory of Organofluorine Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai, ChinaCorrespondence[email protected]
Pages 1803-1808 | Received 04 Dec 2004, Published online: 15 Aug 2006
 
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Abstract

Water‐soluble fullerenol was conveniently synthesized via the direct solvent‐free reaction of fullerene with a mixture of H2O2 and NaOH under grinding conditions in air at room temperature. This practical method provides a novel and efficient access to water‐soluble fullerenol in excellent yield.

Acknowledgments

The authors thank the National Natural Science Foundation of China (NNSFC) (No. 20372077) and Innovation Foundation of Chinese Academy of Sciences for financial support.

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