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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 35, 2005 - Issue 15
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Original Articles

Convenient Preparation of Diethyl (2‐Thienyl)methanephosphonate

Matthew C. Davis Chemistry and Materials Division, Michelson Laboratory, Naval Air Warfare Center, China Lake, California, USACorrespondence[email protected]
Pages 2079-2083 | Received 28 Mar 2005, Published online: 16 Aug 2006
 
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Abstract

This article describes a convenient preparation of diethyl (2‐thienyl)methanephosphonate in 88% overall yield.

Acknowledgments

Financial support from the Office of Naval Research is gratefully acknowledged. M. C. D. thanks several people in NAWCWD: Geoffrey A. Lindsay for advice and encouragement throughout the course of this work; Robert D. Chapman and Andrew P. Chafin for proofreading this manuscript; and librarian Patricia Backes for help finding the federal emission standards.

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