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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 35, 2005 - Issue 15
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Original Articles

Preparation of Methyl N‐Substituted Carbamates from Amides through N‐Chloroamides

Gene A. Hiegel Department of Chemistry and Biochemistry, California State University, Fullerton, California, USACorrespondence[email protected]
&
Tyrone J. Hogenauer Department of Chemistry and Biochemistry, California State University, Fullerton, California, USA
Pages 2091-2098 | Received 28 Mar 2005, Published online: 16 Aug 2006
 
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Abstract

Amides are chlorinated on the nitrogen using trichloroisocyanuric acid, and the N‐chloroamides are then rearranged to the corresponding methyl N‐substituted carbamates by sodium methoxide in methanol.

Acknowledgment

This research was supported in part by a grant from the CSU Special Fund for Research, Scholarship, and Creative Activity.

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