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Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry Volume 32, 2002 - Issue 5
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Original Articles

SYNTHESIS AND CHARACTERIZATION OF TRANSITION METAL TERNARY COMPLEXES OF GLYOXYLIC ACID THIOSEMICARBAZONE AND 4,5-DIAZAFLUOREN-9-ONE

Laijin Tian Department of Chemistry, Qufu Normal University, Qufu, Shandong, 273165, People's Republic of China; Department of Chemistry, Zhejiang University, Hangzhou, 310027, People's Republic of ChinaCorrespondence[email protected]
,
Bin Zhao Department of Chemistry, Qufu Normal University, Qufu, Shandong, 273165, People's Republic of China
,
Zhengyu Zhou Department of Chemistry, Qufu Normal University, Qufu, Shandong, 273165, People's Republic of China
,
Qingsen Yu Department of Chemistry, Zhejiang University, Hangzhou, 310027, People's Republic of China
&
Wentao Yu The State Key Laboratory of Crystal Materials, Shandong University, Jinan, 250100, People's Republic of China
Pages 939-947 | Received 17 Jul 2001, Accepted 14 Mar 2002, Published online: 20 Aug 2006
 
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ABSTRACT

A series of transition metal ternary complexes of glyoxylic acid thiosemicarbazone and 4,5-diazafluoren-9-one were prepared and characterized by elemental analyses, conductivity and magnetic susceptibility measurements,IR, 1H NMR and electronic spectra. Octahedral geometry for the complexes is suggested.

ACKNOWLEDGMENTS

This work was supported by the State Key Laboratory of Crystal Materials and the Natural Science Foundation of Shandong Province.

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