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Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry Volume 34, 2004 - Issue 4
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Original Articles

Zn(II) and Pd(II) Complexes of Thiosemicarbazone‐S‐alkyl Esters Derived from 2/3‐Formylpyridine

İrfan Kızılcıklı Department of Chemistry, Engineering Faculty, Istanbul University, 34850, Avcilar, Istanbul, Turkey
,
Bahri Ülküseven Department of Chemistry, Engineering Faculty, Istanbul University, 34850, Avcilar, Istanbul, TurkeyCorrespondence[email protected]
,
Yasemin Daşdemir Department of Chemistry, Engineering Faculty, Istanbul University, 34850, Avcilar, Istanbul, Turkey
&
Barbaros Akkurt Department of Chemistry, Engineering Faculty, Istanbul University, 34850, Avcilar, Istanbul, Turkey
Pages 653-665 | Received 10 Apr 2003, Accepted 28 Dec 2003, Published online: 16 Nov 2010
 
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Abstract

Representative S‐methyl/ethyl‐4‐H/phenylthiosemicarbazones and their Zn(II) and Pd(II) complexes were synthesized. Characterization of the 1:1 complexes, [Zn(L)Cl2], [Pd(L)Cl2], and [Pd(L)Cl]Cl, was accomplished by means of elemental analyses, IR and 1H NMR spectra. The multidentate S‐alkyl thiosemicarbazones coordinate as mono‐, bi‐, or tridentate ligands depending on the types of the alkyl moiety and metal ion.

Acknowledgment

This study was supported by the Research Fund of Istanbul University, Project Number 1162/070998.

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