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Original Articles

Template Synthesis of Fe(III) and Cr(III) Acyclic Complexes Derived from Diacetyl or Benzil and 1‐Amino‐5‐benzoyl‐4‐phenyl‐1H‐pyrimidine‐2‐one

Pages 733-741 | Received 24 Apr 2003, Accepted 10 Jan 2004, Published online: 16 Nov 2010
 

Abstract

The template synthesis of diacetyl or benzil and 1‐amino‐5‐benzoyl‐4‐phenyl‐1H‐pyrimidine‐2‐one in the presence of Fe(III) and Cr(III) results in the formation of acyclic complexes of the types [ML1X2]X, [ML2X2]X, and [Fe2(L1)2Cl4]Cl2 · H2O, where M = Fe(III), Cr(III), L1 (benzyl derivative), or L2 (diacetyl derivative) are N2O2/ONO acyclic ligands and X = Cl, NO3). The complexes have been characterized by elemental analyses, molar conductance, magnetic measurements, IR, and UV/VIS spectral studies.

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