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International Materials Reviews Volume 49, 2004 - Issue 3-4
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Review Article

Chemically prepared magnetic nanoparticles

M.A. Willard
,
L.K. Kurihara
,
E.E. Carpenter
,
S. Calvin
&
V.G. Harris
Pages 125-170 | Published online: 18 Jul 2013
 
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Abstract

Nanotechnology has spurred efforts to design and produce nanoscale components for incorporation into devices. Magnetic nanoparticles are an important class of functional materials, possessing unique magnetic properties due to their reduced size (below 100 nm) with potential for use in devices with reduced dimensions. Recent advances in processing by chemical synthesis and the characterisation of magnetic nanoparticles are the focus of this review. Emphasis has been placed on the various solution chemistry techniques used to synthesise particles, including: precipitation, borohydride reduction, hydrothermal, reverse micelles, polyol, sol–gel, thermolysis, photolysis, sonolysis, multisynthesis processing and electrochemical techniques. The challenges and methods for examining the structural, morphological, and magnetic properties of these materials are described.

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Hydrothermal synthesis and characterization of nanocrystalline Fe3O4 powders
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Observations of exchange resonance modes on submicrometer sized ferromagnetic particles
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The exchange-spring magnet: a new material principle for permanent magnets
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Amorphous and nanocrystalline materials for applications as soft magnets
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Synthesis of strontium ferrite nanoparticles by coprecipitation in the presence of polyacrylic acid
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Defective iron-oxide nanoparticles synthesised by high temperature plasma processing: a magnetic characterisation versus temperature.
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Synthesis and chemical reactivity of polyol prepared monodisperse nickel powders
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Oxidation of iron in iron/gold core/shell nanoparticles
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Microemulsion processing of manganese zinc ferrites
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Synthesis of nickel ferrite nanoparticles by sol-gel method
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Control of the Size of Cobalt Ferrite Magnetic Fluids: Mössbauer Spectroscopy
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Atomic force microscopy investigation of the surface topography and adhesion of nickel nanoparticles to submicrospherical silica
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Surface Spectroscopic Study of Carbon Monoxide Adsorption on Nanoscale Nickel Colloids Prepared from a Zerovalent Organometallic Precursor
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Synthesis of ultrafine Fe3O4 powder by glycothermal process
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Colloidal synthesis of nanocrystals and nanocrystal superlattices
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Cobalt-based anisotropic particles prepared by the polyol process
Source: Royal Society of Chemistry (RSC)
Investigations into the Phase Behavior of Nonionic Ethoxylated Surfactants Using 2H NMR Spectroscopy
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Preparation and magnetic properties of barium hexaferrite nanoparticles produced by the citrate process
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Processing and cation redistribution of MnZn ferrites via high-energy ball milling
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Microstructural characterisation of Ni, Co and NiCo fine powders for physical sensors☆
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Electron spin resonance investigation of Mn–Zn ionic ferrofluid
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Influence of pH on the composition and structure of Fe-Co-B alloy particles prepared by borohydride reduction in aqueous solutions
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Size-Selective Electrodeposition of Mesoscale Metal Particles in the Uncoupled Limit
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Nonstoichiometric Zinc Ferrite Nanocrystals: Syntheses and Unusual Magnetic Properties
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Magnetic and structural properties of ultrafine CoFe1.9RE0.1O4 (Re=Gd, Nd) powders grown by using a sol-gel method
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Magnetization curling in superparamagnetic spheres
Source: American Physical Society (APS)
Synthesis of Cubic Antiferromagnetic KMnF3 Nanoparticles Using Reverse Micelles and Their Self‐Assembly
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Hydrothermal synthesis of manganese zinc ferrites
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Chain-of-cubes iron nanoparticles prepared by borohydride reduction of acicular akaganeite particles
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Atomic structure and magnetic properties of MnFe2O4 nanoparticles produced by reverse micelle synthesis
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Microstructure and Magnetic Properties of Fe(C) and Fe(O) Nanoparticles
Source: American Chemical Society (ACS)
Mechanism of the Shape and Structure Control of Monodispersed α-Fe2O3Particles by Sulfate Ions
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Sonochemical Synthesis and Characterization of Nanometer-Size Transition Metal Oxides from Metal Acetates
Source: American Chemical Society (ACS)
Magnetic properties of nano-crystalline Gd- or Pr-substituted CoFe2O4 synthesized by the citrate precursor technique
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Synthesis and characterization of nanophasic goethite
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Further consideration of hydrothermal synthesis of barium ferrite fine particles
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Magnetic properties of iron and iron platinum alloys synthesized via microemulsion techniques
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Synthesis, Crystal Structure, and Magnetic Properties of ϵ‐InxFe2–xO3 Nanorod‐Shaped Magnets
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Synthesis of very fine maghemite particles
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Sonochemical synthesis of nanostructured catalysts
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Mixed spinel structure in nanocrystalline NiFe 2 O 4
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Preparation of magnetic cobalt fibres and their microwave properties
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Switching behaviour of single nanowires inside dense nickel nanowire arrays
Source: Institute of Electrical and Electronics Engineers (IEEE)
Surface anisotropy in ferromagnetic nanoparticles
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Theory, Production and Mechanism of Formation of Monodispersed Hydrosols
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Polyhedral Shapes of Cobalt Nanocrystals and Their Effect on Ordered Nanocrystal Assembly
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Site specification on normal and magnetic XANES of ferrimagnetic Fe3O4 by means of resonant magnetic Bragg scattering
Source: International Union of Crystallography (IUCr)
Fabrication and Characterization of the Plate-Shaped γ-Fe2O3 Nanocrystals
Source: American Chemical Society (ACS)
Colloidal Synthesis and Self-Assembly of CoPt3 Nanocrystals
Source: American Chemical Society (ACS)
Magnetic properties of Co-Ni spinel ferrite fine particles with high coercivity prepared by the chemical coprecipitation method
Source: Institute of Electrical and Electronics Engineers (IEEE)
CoPt and FePt nanowires by electrodeposition
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Sodium borohydride reduction of aqueous iron–zirconium solutions: chemical routes to amorphous and nanocrystalline Fe–Zr–B alloys
Source: Royal Society of Chemistry (RSC)
Structural and magnetic properties of polymer-stabilized tetragonal Ni nanoparticles
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Survey of conditions to produce metal–boron amorphous and nanocrystalline alloys by chemical reduction
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Sonochemical preparation of nanosized amorphous Fe-Ni alloys
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Electrochemical Synthesis for the Control of γ-Fe2O3 Nanoparticle Size. Morphology, Microstructure, and Magnetic Behavior
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Potbellies, wasp-waists, and superparamagnetism in magnetic hysteresis
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Spin canting and size effects in nanoparticles of nonstoichiometric cobalt ferrite
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Structure and magnetic properties of nanostructured Ni-ferrite
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SYNTHESIS, SELF-ASSEMBLY, AND MAGNETIC PROPERTIES OF FEXCOYPT100-X-Y NANOPARTICLES
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Preparation and properties of magnetic nano-and microsized particles for biological and environmental separations
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Organometallic synthesis and magnetic properties of ferromagnetic Sm–Co nanoclusters
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Crystalline, Shape, and Surface Anisotropy in Two Crystal Morphologies of Superparamagnetic Cobalt Nanoparticles by Ferromagnetic Resonance
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New aqueous magnetic fluids
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Preparation and properties of monodisperse magnetic fluids
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Synthesis of magnetic spinel ferrite CoFe2O4 nanoparticles from ferric salt and characterization of the size-dependent superparamagnetic properties
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Lithium ferrite nanoparticles for ferrofluid applications
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Pd-coated Ni nanoparticles by the polyol method: an efficient hydrogenation catalyst
Source: Royal Society of Chemistry (RSC)
Structure determination of small particles by HREM imaging: Theory and experiment
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Synthesis and Magnetic Characterization of Zinc Ferrite Nanoparticles with Different Environments: Powder, Colloidal Solution, and Zinc Ferrite−Silica Core−Shell Nanoparticles
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Kinetics of producing barium hexaferrite in a low alkaline concentration by hydrothermal method
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Interpretation of High Coercivity in Ferromagnetic Materials
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Evolution in the structure of akaganeite and hematite during hydrothermal growth: An in situ synchrotron X-ray diffraction analysis
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Detection of a micron-sized magnetic sphere using a ring-shaped anisotropic magnetoresistance-based sensor: A model for a magnetoresistance-based biosensor
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Self-Organization of Magnetic Nanosized Cobalt Particles**
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Synthesis of nanosize metallic and alloyed particles in ordered phases
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Nanocrystalline metallic powders and films produced by the polyol method
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Fe(Me2-bpy)2(NCSe)2 spin-crossover micro- and nanoparticles showing spin-state switching above 250 K
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Barium ferrite powders obtained by co-precipitation
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Size-dependent structural and magnetic properties of chemically synthesized Co-Ni-Ga nanoparticles
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Anomalous Electroless Polyol Deposition of FeNi Powders and Films
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Synthesis and Characterization of CoO, Co3O4, and Mixed Co/CoO Nanoparticules
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Low temperature synthesis of Ni0.8Zn0.2Fe2O4 powder and its characterization
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Single Electron Tunneling Through Nano‐Sized Cobalt Particles
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Magnetic properties of CoFe2O4 powders and thin films grown by a sol-gel method
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Synthesis, Characterization, and Magnetic Properties of Cobalt Nanoparticles from an Organometallic Precursor
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The effects of mechanical activation in synthesizing ultrafine barium ferrite powders from co-precipitated precursors
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Co-Pt-B particles prepared by chemical reduction
Source: Institute of Electrical and Electronics Engineers (IEEE)
Nanoparticles of nickel and silver produced by the polyol reduction of the metal salts intercalated in montmorillonite
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Cobalt-ferrite nanoparticles: correlations between synthesis procedures, structural characteristics and magnetic properties
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Compositionally controlled FePt nanoparticle materials
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The adsorption of monolayer coatings on iron nanoparticles: Mössbauer spectroscopy and XANES results
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Hydrothermal Synthesis of Manganese Zinc Ferrite Powders from Oxides
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Hydrothermal Synthesis of Molybdenum Oxide Based Materials: Strategy and Structural Chemistry
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Hysteresis Loops of Mixtures of Ferromagnetic Micropowders
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Scalable synthesis of dispersible iron carbide (Fe3C) nanoparticles by ‘nanocasting’
Source: Royal Society of Chemistry (RSC)
Sonochemical preparation of amorphous nickel
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Effect of the pH on the microstructure and magnetic properties of electrodeposited cobalt nanowires
Source: Institute of Electrical and Electronics Engineers (IEEE)
Synthesis and characterization of anisometric cobalt nanoclusters.
Source: American Association for the Advancement of Science (AAAS)
Heterogeneous nucleation and growth of metal nanoparticles in polyols
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ORGANOMETALLIC COMPOUNDS AS SINGLE-SOURCE PRECURSORS TO NANOCOMPOSITE MATERIALS : AN OVERVIEW
Source: Elsevier BV
Local magnetic properties of nanocrystalline Ni and Pd-Fe
Source: Elsevier BV
Recent advances in multifunctional magnetic nanoparticles and applications to biomedical diagnosis and treatment
Source: Royal Society of Chemistry (RSC)
Magnetic relaxation of iron nanoparticles
Source: AIP Publishing
Quantitative speciation of Mn-bearing particulates emitted from Autos burning (methylcyclopentadienyl)manganese tricarbonyl-added gasolines using XANES spectroscopy
Source: American Chemical Society (ACS)
Nanosize cobalt boride particles: Control of the size and properties
Source: Elsevier BV
Novel Synthesis of Monodispersed Pd/Ni Nanoparticles
Source: American Chemical Society (ACS)
Sonochemical Synthesis of Iron Colloids
Source: American Chemical Society (ACS)
Synthesis of biogenic hematite (α-Fe2O3) nanoparticles for antibacterial and nanofluid applications
Source: Royal Society of Chemistry (RSC)
Magnetization temperature dependence in iron nanoparticles
Source: American Physical Society (APS)
Physical Theory of Ferromagnetic Domains
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Ultrafine metal particles
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Iron-oxide-based nanoparticles produced by pulsed infrared laser pyrolysis of Fe(CO)5
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Nanoparticles of Barium Hexaferrite by Gel to Crystallite Conversion and their Magnetic Properties
Source: Springer Science and Business Media LLC
Micellar factors which play a role in the control of the nanosize particles of cobalt ferrite
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Increased Cellular Uptake of Biocompatible Superparamagnetic Iron Oxide Nanoparticles into Malignant Cells by an External Magnetic Field
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Theory of multicomponent micelles and microemulsions
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Binding Parameters of Magnetite Nanoparticles Interaction with Anticancer Drug Doxorubicin
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Self-Assembled Monolayer Coatings on Amorphous Iron and Iron Oxide Nanoparticles: Thermal Stability and Chemical Reactivity Studies
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Preparation of nanocomposites containing iron and nickel–zinc ferrite
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X-ray absorption spectra and X-ray magnetic circular dichroism studies at Fe and Co L2,3 edges of mixed cobalt-zinc ferrite nanoparticles : cationic repartition, magnetic structure and hysteresis cycles
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In situ energy dispersive EXAFS (EDE) of low loaded Pt(acac)2/HI SiO2 catalyst precursors on a timescale of seconds and below
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Domain Shapes and Superlattices Made of Cobalt Nanocrystals
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Ordered Two‐Dimensional Arrays of Ferrite Nanoparticles
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Thermal variation of the relaxation time of the magnetic moment of gamma -Fe2O3 nanoparticles with interparticle interactions of various strengths.
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Activated carbon doped WO 3 for photocatalytic degradation of rhodamine-B
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Particle size effects on magnetic properties of yttrium iron garnets prepared by a sol-gel method
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Improving the magnetic properties of hydrothermally synthesized barium ferrite
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Determination of crystallite size in a magnetic nanocomposite using extended x-ray absorption fine structure
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Structural, morphological, and magnetic study of nanocrystalline cobalt-copper powders synthesized by the polyol process
Source: Springer Science and Business Media LLC
Magnetic Nanomaterials for Magnetically-Aided Drug Delivery and Hyperthermia
Source: MDPI AG
X-ray absorption, neutron diffraction, and Mössbauer effect studies of MnZn–ferrite processed through high-energy ball milling
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Ordered Self-Assembling of Tetrahedral Oxide Nanocrystals
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Multiresponsive Poly(N-Acryloyl glycine)-Based Nanocomposite and Its Drug Release Characteristics
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5-Fluorouracil-loaded β-cyclodextrin-carrying polymeric poly(methylmethacrylate)-coated samarium ferrite nanoparticles and their anticancer activity
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Dynamic Light Scattering Measurement of Nanometer Particles in Liquids
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Preparation of acicular /spl alpha/-Fe nanoparticles in tubular lecithin colloids
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The kinetics of precipitation of barium sulfate from aqueous solution
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Enhanced magnetization of nanoscale colloidal cobalt particles.
Source: American Physical Society (APS)
Preparation and characterization of polymer-protected PtCo bimetallic colloids and their catalytic properties in the selective hydrogenation of cinnamaldehyde
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Magnetic properties of arrays of interacting Co nanocrystals
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Nanostructures of gold coated iron core-shell nanoparticles and the nanobands assembled under magnetic field
Source: Springer Science and Business Media LLC
Shape Control of Thermodynamically Stable Cobalt Nanorods through Organometallic Chemistry
Source: Wiley
Determination of the Mo surface environment of Mo/TiO2 catalysts by EXAFS, XANES and PCA
Source: Springer Science and Business Media LLC
Magnetic properties of microemulsion synthesized cobalt fine particles
Source: AIP Publishing
A novel technique by the citrate pyrolysis for preparation of iron oxide nanoparticles
Source: Elsevier BV
Preparation of nanoscale iron and Fe3O4 powders in a polymer matrix
Source: Springer Science and Business Media LLC
Synthesis of colloidal cobalt nanoparticles with controlled size and shapes
Source: Springer Science and Business Media LLC
Size-Controlled Synthesis of Magnetite Nanoparticles
Source: American Chemical Society (ACS)
Use of Surfactant Micelles to Control the Structural Phase of Nanosize Iron Clusters
Source: American Chemical Society (ACS)
Physical synthesis of iron oxide nanoparticles and their biological activity in vivo
Source: Springer Science and Business Media LLC
Nanoscale Bimetallic CoxPt1-x Particles Dispersed in Poly(vinylpyrrolidone): Synthesis from Organometallic Precursors and Characterization
Source: American Chemical Society (ACS)
Phase Transformation, Coalescence, and Twinning of Monodisperse FePt Nanocrystals
Source: American Chemical Society (ACS)
Magnetic Properties of Nanostructured Materials
Source: American Chemical Society (ACS)
Temperature Dependence of the Magnetization of Disc Shaped NiO Nanoparticles
Source: Wiley
In Situ X-ray Absorption Spectroscopy Studies on Chemical Oscillations in the CO/O2 System on Supported Pd Catalysts
Source: American Chemical Society (ACS)
Recent progress in electron probe microanalysis
Source: IOP Publishing
Sonochemical Preparation of Nanosized Amorphous NiFe2O4 Particles
Source: American Chemical Society (ACS)
Synthesis of inorganic compounds (metal, oxide and hydroxide) in polyol medium: A versatile route related to the sol-gel process
Source: Springer Science and Business Media LLC
Magnetic Nanoparticles: From Design and Synthesis to Real World Applications
Source: MDPI AG
Superparamagnetism
Source: AIP Publishing
Deciphering magnetic hyperthermia properties of compositionally and morphologically modulated FeNi nanoparticles using first-order reversal curve analysis.
Source: IOP Publishing
Exchange-coupled nanocomposite magnets by nanoparticle self-assembly
Source: Springer Science and Business Media LLC
A Mechanism of Magnetic Hysteresis in Heterogeneous Alloys
Source: The Royal Society
Magnetic properties of nanosized wires
Source: AIP Publishing

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