Microstructural, mechanical and electrochemical characterisation of biomaterial ASTM F745 cast by vacuum

Abstract

Countergravity low pressure casting (CLA) was performed to enhance the properties of ASTM F745 stainless steel (SS), which is usually used as biomaterial. The macro- and microstructures were compared with those obtained by the conventional process of investment casting (IC). The SS cast by CLA (SSCLA) exhibited a smaller size of solidification cell and finer dendritic microstructure. The average of its dendritic primary spacing was 110·4 μm, while for the same steel cast by IC (SSIC), it was 186·7 μm. The density of non-metallic inclusions δ_I in the SSCLA was 717 I mm⁻², being the majority of them smaller than 1·5 μm. In the case of SSIC, δ_I was 852 I mm⁻², with a size distribution of up to 8 μm. The SSCLA showed a higher breakdown potential than the SSIC, the values being 0·300 and 0·210 V(saturated calomel electrode) respectively, which means a higher resistance to suffer localised corrosion. Finely, the CLA process also allowed obtaining better mechanical properties.

Keywords:

• Biomaterials
• Austenitic steel
• Vacuum casting
• Mechanical properties
• Corrosion

The authors thank the Comisión de Investigaciones Científicas de la Provincia de Buenos Aires (CICPBA), the Consejo Nacional de Investigaciones Científicas y Técnicas (CONICET) and the Universidad Nacional de La Plata of Argentina for the financial support to carry out the present research paper.