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Abstract
For the first time, electroless nickel plated ZrO2 (Ni-NCZ) particles were used for the co-electrodeposition of Ni-NCZ composite coating. Optical microscope, SEM and X-ray diffraction studies showed that Ni-NCZ has a rough surface with a smaller Ni crystallite size than Ni-ZrO2 due to the conductive properties of NCZ particles, which provide more nucleation sites for Ni clusters. The energy dispersive X-ray spectroscopy measurement results showed that Ni-NCZ has more co-electrodeposited particles than Ni-ZrO2. This is due to the more positive zeta potential of NCZ particles compared to that of ZrO2. The microhardness measurements demonstrated that the Ni-NCZ composite coating has a higher microhardness than Ni-ZrO2 due to the higher amounts of co-electrodeposited particles and lower crystallite size. Electrochemical impedance spectroscopy and potentiodynamic polarisation test showed that the corrosion resistance of Ni-NCZ is higher than that of Ni-ZrO2.