Filler morphology of resin-based low-viscosity materials and surface properties after several photoactivation times

Abstract

Aim. This study aimed to characterize the morphology of filler particles and to analyze the effect of shortened and extended photoactivation times on hardness (VHN) and cross-link density (CLD) of resin-based low-viscosity materials. Methods. Sixteen commercially available materials were tested: four fissure sealants (Alpha Seal, Fluroshield Yellowed, Bioseal and Fluroshield White) and 12 flowable composites (Opallis T, Permaflo T, Opallis A2, Natural Flow A2, Master Flow A2, Permaflo A2, Filtek Z350 A2, Natural Flow O, Master Flow OA2, Opallis OA3.5, Filtek Z350 OA3, Opallis OP) at six curing times (10 s, 20 s, 30 s, 40 s, 50 s and 60 s). Specimens were fabricated (n = 5), analyzed by Scanning Electron Microscopy, by VHN and by CLD. Results. Unimodal and multimodal filler particles sizes with spherical and irregular shapes were observed. Unfilled materials were also detected. There were no differences among curing times for either VHN or CLD. Opallis A2 and Opallis OA3.5 showed the highest VHN at all curing times, whereas Master Flow A2 and Master Flow OA2 presented the lowest VHN. Opallis A2 presented the highest CLD at all curing times and Alpha Seal showed the lowest CLD. Conclusions. Filler particle morphology differed among the resin-based low-viscosity materials tested. The shortest photoactivation time tested could yield similar VHN and CLD means to those provided by the most extended photoactivation time.

Key Words::

• flowable hybrid composite
• physical properties
• pit and fissure sealants

Acknowledgments

The authors thank Vigodent (Rio de Janeiro, RJ, Brazil), FGM (Joinville, SC, Brazil), DFL (Rio de Janeiro, RJ, Brazil) and Biodinâmica (Ibiporã, PR, Brazil) for providing some materials and the curing-light unit used in this study. The authors also show gratitude to NEPGN (Petroleum and Natural Gas Research Center) and to CTPETRO-INFRA I and FINEP/LIEM projects for SEM assistance.

Declaration of interest: The authors report no conflicts of interest. The authors alone are responsible for the content and writing of the paper.