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Agricultural and Biological Chemistry Volume 53, 1989 - Issue 11
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Organic Chemistry

Reinvestigation of the Reduction of Di- and Trihydroxyphenylalkanones with Sodium Borohydride in an Aqueous Alkali

Takakazu FunatsuDepartment of Bioscience and Biotechnology, Faculty of Agriculture, Shinshu University, Minamiminowa 8304, Kamiina, Nagano 399–45, Japan
,
Ryozo IriyeDepartment of Bioscience and Biotechnology, Faculty of Agriculture, Shinshu University, Minamiminowa 8304, Kamiina, Nagano 399–45, Japan
,
Hideyuki TakaiDepartment of Bioscience and Biotechnology, Faculty of Agriculture, Shinshu University, Minamiminowa 8304, Kamiina, Nagano 399–45, Japan
&
Mitsuru HirotaDepartment of Bioscience and Biotechnology, Faculty of Agriculture, Shinshu University, Minamiminowa 8304, Kamiina, Nagano 399–45, Japan
Pages 3087-3089 | Received 07 Jun 1989, Published online: 08 Sep 2014

References and Notes

  • K. H. Bell, Aust. J. Chem., 22, 601 (1969).
  • J. B. Harbone, T. J. Mabry and H. Mabry, “The Flavonoids,” Chapmann and Hall, London, 1975, p. 496.
  • 2,4,6-Trihydroxypropiophenone (6) yielded phlorog-lucinol (5) and propanoic acid (7) in a quantitative yield by treating with 1 N-NaOH solution at 100°C, while 2,4-dihydroxyacetophenone (9) was stable under these conditions.
  • D. J. Cram and F. W. Cranz, J. Am. Chem. Soc., 72, 595 (1950).

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