Validation of an HPLC Analytical Method for Determination of Pancuronium Bromide in Pharmaceutical Injections

REFERENCES

• Andersen , B.D. , Alcaraz , A. , and Grant , P.M. 2005 . Pancuronium bromide (Pavulon) isolation and identification in aged autopsy tissues and fluids . J. Forensic Sci. , 50 : 196 – 203 .
   PubMed Web of Science ®Google Scholar
• Association of Official Analytical Chemists International . 2003 . Official Methods of Analytical Chemists of AOAC International , 17th ed., XX .
   Google Scholar
• Aubeck , R. , Bräuchle , C. , and Hampp , N. 1990 . Íon selective membrane electrodes for the determination of the muscle relaxants pancuronium, tubocurarine, gallamine and succinylcholine . Anal. Chim. Acta. , 238 : 405 – 410 .
   Web of Science ®Google Scholar
• Ballard , K.D. , Vickery , W.E. , Nguyen L.T. , and Diamond , F.X. 2006 . An analytical strategy for quaternary ammonium neuromuscular blocking agents in a forensic setting using LC-MS/MS on a tandem quadrupole/time-of-flight instrument . J. Am. Soc. Mass Spectrom. , 17 : 1457 – 1469 .
   PubMed Web of Science ®Google Scholar
• Briglia , E.J. , Davis , P.L. , Katz , M. , and Dal Cortivo , L.A. 1990 . Attempted murder with pancuronium . J. Forensic Sci. , 35 : 1468 – 1476 .
   PubMed Web of Science ®Google Scholar
• British Pharmacopoeia, sixth edition , 2008 . vol. 3 .
   Google Scholar
• Cirimele , V. , Villain , M. , Pépin , G. , Ludes , B. , and Kintz , P. 2003 . Screening procedure for eight quaternary nitrogen muscle relaxants in blood by high-performance liquid chromatography–electrospray ionization mass spectrometry . J. Chromatogr. B. , 789 : 107 – 113 .
   PubMed Web of Science ®Google Scholar
• Furuta , T. , Canfell , P.C. , Castagnoli , K.P. , Sharma , M.L. , and Miller , R.D. 1988 . Quantitation of pancuronium, 3-desacetylpancuronium, vecuronium, 3-desacetylvecuronium, pipecuronium and 3-desacetylpipecuronium in biological fluids by capillary gas chromatography using nitrogensensitive detection . J. Chromatogr. , 427 : 41 – 53 .
   PubMed Web of Science ®Google Scholar
• Gazdag , M. , Babják , M. , Kemenes-Bakos , P. , and Görög , S. 1991 . Ion-pair high-performance liquid chromatographic separation of quaternary ammonium steroids on silica . J. Chromatogr. , 550 : 639 – 644 .
   PubMed Web of Science ®Google Scholar
• Gazdag , M. , Szepesi , G. , Varsányi , K. , Végh , Z. , and Pap-Sziklay , Z. 1985 . Chromatography of bis-quaternary amino steroids. I. Separation on sílica by thin-layer and high-performance liquid chromatography . J. Chromatogr. , 328 : 279 – 287 .
   Web of Science ®Google Scholar
• Gazdag , M. , Varsányi , K. , and Zsepesi , G. 1985 . Chromatography of bis-quaternary amino steroids. II. Separation on chemically bonded sílica phases . J. Chromatogr. , 347 : 284 – 290 .
   Web of Science ®Google Scholar
• International Conference on Harmonization . 2005 . Validation of Analytical Procedures: Text and Methodology Q2(R1) .
   Google Scholar
• Kała , M. and W. Lechowicz . 2004 . Instability of pancuronium in postmortem blood and liver taken after a fatal intramuscular Pavulon injection . Foren. Sci. Int. , 143 : 191 – 198 .
   PubMed Web of Science ®Google Scholar
• Kersten , U.W. , Meijer , D.K.F. , and Agoston , S. 1973 . Fluorimetric and chromatographic determination of pancuronium bromide and its metabolites in biological materials . Clin. Chim. Acta. , 44 : 59 – 66 .
   PubMed Web of Science ®Google Scholar
• Kinget , R. and Michoel , A. 1976a . Thin layer chromatography of pancuronium bromide and its hydrolysis products . J. Chromatogr. , 120 : 234 – 238 .
   PubMed Web of Science ®Google Scholar
• Kinget , R. and Michoel , A. 1976b. A. Kinetic study of the hydrolysis of pancuronium bromide. II specific and general base catalysis. Acta Pharm. Suec. , 13: 321–330.
   PubMedGoogle Scholar
• McKenzie , A.G. 2000 . Prelude to pancuronium and vecuronium . Anaesthesia. , 55 : 551 – 556 .
   PubMed Web of Science ®Google Scholar
• Meier , P.C. and Zünd , R.E. 2000 . Statistical Methods in Analytical Chemistry, , 2nd. ed . New York : John Wiley & Sons .
   Google Scholar
• Michoel A. and Kinget , R. 1976 . Kinetic study of the hydrolysis of pancuronium bromide. I specific acid catalysis . Acta Pharm. Suec. , 13 : 267 – 276 .
   PubMedGoogle Scholar
• Miller , J.N. and Miller , J.C. 2002 . Estadística y quimiometría para química analítica. , 4th. ed . Madrid : Prentice Hall .
   Google Scholar
• Rawlings , J.O. , Pantula , S.G. , and Dickey , D.A. 1998 . Applied Regression Analysis. , 2nd. ed . New York : Springer .
   Google Scholar
• Sayer , H. , Quintela , O. , Marquet , P. , Dupuy , J. , Gaulier , J. , and Lachâtre , G. 2004 . Identification and quantitation of six non-depolarizing neuromuscular blocking agents by LC–MS in biological fluids . J. Anal. Toxicol. , 28 : 105 – 110 .
   PubMed Web of Science ®Google Scholar
• Stankov-Jovanović , V.P. , Nikolić-Mandić , S.D. , Mandić , L.M. , and Mitić , V.D. 2006 . Cholinesterase inhibition based determination of pancuronium bromide in biological samples . Anal. Bioanal. Chem. , 385 : 1462 – 1469 .
   PubMed Web of Science ®Google Scholar
• Tanaka , K. , Hioki , M. , and Shindo , H. 1974 . Determination of pancuronium bromide and its metabolites in human urine by dye-extraction method-relation between the extractability and structure of quaternary ammonium ions . Chem. Pharm. Bull. , 22 : 2599 – 2606 .
   PubMed Web of Science ®Google Scholar
• Wingard , L.B. , Abouleish , E. , West , D.C. , and Goehl , T.J. 1979 . Modified fluorometric quantitation of pancuronium bromide and metabolites in human material and umbilical serums . J. Pharm. Sci. , 68 : 914 – 915 .
   PubMed Web of Science ®Google Scholar
• Zecevic , M. , Zivanovic , L. , and Stojkovic , A. 2002 . Validation of a high-performance liquid chromatography method for the determination of pancuronium in Pavulon injections . J. Chromatogr. A. , 949 : 61 – 64 .
   PubMed Web of Science ®Google Scholar