Determination of Gentamicin Sulphate in Injection Solutions by Derivative Spectrophotometry

REFERENCES

• Al-Amoud , A.I. , Clark , B.J. , and Chrystyn , H. 2002 . Determination of gentamicin in urine samples after inhalation by reversed-phase high-performance liquid chromatography using pre-column derivatisation with o-phthalaldehyde . J. Chromatogr. B. , 769 : 89 – 95 .
   PubMed Web of Science ®Google Scholar
• Cherlet , M. , Baere , S.D. , and Backer , P.D. 2000 . Determination of gentamicin in swine and calf tissues by high-performance liquid chromatography combined with electrospray ionization mass spectrometry . J. Mass. Spectr. , 35 : 1342 – 1350 .
   PubMed Web of Science ®Google Scholar
• El-Yazgi , A. 1999 . Simplified high-performance liquid chromatographic method for the determination of gentamicin sulfate in a microsample of plasma: Comparison with fluorescence polarization immunoassay . Therap. Drug Monitor. , 21 : 647 – 652 .
   PubMed Web of Science ®Google Scholar
• European Pharmacopeia, , 4th ed. 2002 . Strasbourg , France : Council of Europe .
   Google Scholar
• Hanes , S.D. and Herring , V.L. 2001 . Gentamicin enzyme-linked immunosorbent assay for microdialysis samples . Therap. Drug Monitor. , 23 : 689 – 693 .
   PubMed Web of Science ®Google Scholar
• Isoherranen , N. and Soback , S. 2000 . Determination of gentamicins C(1), C(1a), and C(2) in plasma and urine by HPLC . Clin. Chem. , 46 : 837 – 842 .
   PubMed Web of Science ®Google Scholar
• Kaale , E. , Leonard , S. , Van Schepdael , A. , Roets , E. , and Hoogmartens , J. 2000 . Capillary electrophoresis analysis of gentamicin sulphate with UV detection after pre-capillary derivatization with 1,2-phthalic dicarboxaldehyde and mercaptoacetic acid . J. Chromatogr. A , 895 : 67 – 79 .
   PubMed Web of Science ®Google Scholar
• Krzek , J. , Stolarczyk , M. , and Rzeszutko , W. 2002 . Spectrophotometric determination of gentamycin sulfate(VI), dexamethasone, and methyl and propyl 4-hydroxybenzoates in pharmaceuticals . Chem. Anal. , (Warsaw) 47 : 299 – 309 .
   Web of Science ®Google Scholar
• Posyniak , A. , Żmudzki , J. , and Niedzielska , J. 2001 . Sample preparation for residue determination of gentamicin and neomicin by liquid chromatography . J. Chromatogr. A , 914 : 59 – 66 .
   PubMed Web of Science ®Google Scholar
• Prasad , P.B.N. , Rao , A.C.S. , Mathur , S.C. , Kumar , Y. , and Talwar , S.K. 1998 . Comparative HPTLC and HPLC studies on quantitative determination of gentamicin sulphate in bulk drugs . Indian Drugs , 35 : 744 – 747 .
   Google Scholar
• Stead , D.A. and Richards , R.M. 1996 . Sensitive fluorimetric determination of gentamicin sulfate in biological matrices using solid-phase extraction, pre-column derivatization with 9-fluorenylmethyl chloroformate and reversed-phase high-performance liquid chromatography . J. Chromatogr. B , 675 : 295 – 302 .
   PubMed Web of Science ®Google Scholar
• Walker , S.E. and Coates , P.E. 1981. High-performance liquid chromatographic methods for determination of gentamicin in biological fluids. J. Chromatogr. A , 223: 131–138.
   PubMed Web of Science ®Google Scholar
• Yusuf , A. , Al-Rawithi , S. , Raines , D. , Frayha , H. , Toonsi , T.A. , Al-Mohsen , I. , and El-Yazgi , A. 1999 . Simplified high-performance liquid chromatographic method for the determination of gentamicin sulfate in a microsample of plasma: Comparison with fluorescence polarization immunoassay . Therapeutic Drug Monitoring , 21 : 647 – 652 .
   PubMed Web of Science ®Google Scholar
• Zejc , A. and Gorczyca , M. 1999 . Drug Chemistry (in Polish), , 2nd ed. PZWL . Warsaw , Poland .
   Google Scholar