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GAS CHROMATOGRAPHY

Simultaneous Extraction and Derivatization of Volatile Organic Acids in Flue-Cured Tobacco with Headspace Solid-Phase Microextraction Followed by GC-MS

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Pages 640-650 | Received 07 Aug 2012, Accepted 10 Sep 2012, Published online: 19 Feb 2013

REFERENCES

  • Abalos , M. , J. M. Bayona , and J. J. Pawliszyn . 2000 . Development of a headspace solid-phase microextraction procedure for the determination of free volatile fatty acids in waste waters . J. Chromatogr. A 873 : 107 – 115 .
  • Chen , Z. Y. , L. L. Luo , Y. Wu , and X. Y. Zeng . 2001 . Determination of organic acids in cigarette smoke . Chin. J. Chromatography 19 : 374 – 377 .
  • Clark , T. J. , and J. E. Bunch . 1997a . Derivatization solid-Phase microextraction gas chromatographic-mass spectrometric determination of organic acids in tobacco . J. Chromatogr. Sci. 35 : 209 – 212 .
  • Clark , T. J. , and J. E. Bunch . 1997b . Qualitative and quantitative analysis of flavor additives on tobacco products using SPME-GC-mass spectroscopy . J. Agric. Food. Chem. 45 : 844 – 849 .
  • Davis , D. L. , and M. T. Nielsen . 1999 . A Review of the Biosynthesis of the Alkaloids of Tobacco . Oxford , UK : Blackwell Science .
  • Guo , L. , H. M. Liu , F. W. Xie , X. D. Zhao , K. Liao , and S. N. Zhang . 2008 . Simultaneous determination of 26 volatile and semi-volatile organic acids in tobacco by GC - MS/SIM . Chin. J. Instrum. Anal. 7 : 739 – 743 .
  • He , Y. , and H. K. Lee . 1997 . Liquid-phase microextraction in a single drop of organic solvent by using a conventional microsyringe . Anal. Chem. 69 : 4634 – 4640 .
  • Jones , T. C. , and I. Schmeltz . 1968 . Fingerprint gas chromatographic analysis of tobacco leaf acids . Tob. Sci. 12 : 11 – 15 .
  • Lin , J. T. , S. C. Liu , Y. C. Shen , and D. J. Yang . 2011 . Comparison of various preparation methods for determination of organic acids in fruit vinegars with a simple ion-exclusion liquid chromatography . Food Anal. Methods 4 : 531 – 539 .
  • Ma , J. P. , W. H. Lu , J. H. Li , Z. W. Song , D. Y. Liu , and L. X. Chen . 2012 . Determination of Geosmin and 2-Methylisoborneol in Water by Headspace Liquid-phase Microextraction Coupled with Gas Chromatography-Mass Spectrometry . Anal. Lett. 44 : 1544 – 1557 .
  • Pérès , C. , C. Viallon , and J. L. Berdagué . 2001 . Solid-phase microextraction-mass spectrometry: a new approach to the rapid characterization of cheeses . Anal. Chem. 73 : 1030 – 1036 .
  • Prosen , H. , and L. Zupancic-Kralj . 1999 . Solid-phase microextraction . TrAC Trends Anal. Chem. 18 : 272 – 282 .
  • Qiu , J. S. 1999 . Statistics aided optimization for high-performance liquid chromatographic analysis of organic acids in tobacco . J. Chromatogr. A 859 : 153 – 158 .
  • Qiu , J. S. , and X. H. Jin . 2002. Development and optimization of organic acid analysis in tobacco with ion chromatography and suppressed conductivity detection. J. Chromatogr. A 950: 81–88.
  • Sádecká , J. , and J. Polonský . 2003 . Determination of organic acids in tobacco by capillary isotachophoresis . J. Chromatogr. A 988 : 161 – 165 .
  • Sarafraz-Yazdi , A. , and A. Amiri . 2010 . Liquid-phase microextraction . TrAC Trends Anal. Chem. 29 : 1 – 14 .
  • Schmeltz , I. , R. L. Stedman , and R. L. Miller . 1963 . Gas chromatography study of the steam volatile fatty acids of various tobaccos . J. Assoc. Offic. Agric. Chemists 46 : 779 – 784 .
  • Sha , Y. F. , J. R. Meng , Y. C. Zhang , C. H. Deng , and D. Wu . 2010 . Determination of volatile organic acids in tobacco by single-drop microextraction with in-syringe derivatization followed by GC-MS . J. Sep. Sci. 33 : 212 – 217 .
  • Sun , S. H. , J. P. Xie , F. W. Xie , and Z. Y. Zong . 2008 . Determination of volatile organic acids in oriental tobacco by needle-based derivatization headspace liquid-phase microextraction coupled to gas chromatography/mass spectrometry . J. Chromatogr. A 1179 : 89 – 95 .
  • Tso , T. C. 1991 . Production, Physiology, and Biochemistry of Tobacco Plant . Beltsville , MD : Ideals Inc.
  • Wang , B. X. , S. H. Yang , G. H. Chen , Y. Wu , Y. Hou , and G. W. Xu . 2008 . Simultaneous determination of non-volatile, semi-volatile, and volatile organic acids in tobacco by SIM-Scan mode GC-MS . J. Sep. Sci. 31 : 721 – 726 .
  • Wu , W. J. , D. L. Ashley , and C. H. Watson . 2002 . Determination of nicotine and other minor alkaloids in international cigarettes by solid-phase microextraction and gas chromatography/mass spectrometry . Anal. Chem. 74 : 4878 – 4884 .
  • Yang , M. H. , and Y. M. Choong . 2001 . A rapid gas chromatographic method for direct determination of short-chain (C2–C12) volatile organic acids in foods . Food Chem. 75 : 101 – 108 .
  • Zachariadis , G. A. , and A. V. Langioli . 2012 . Headspace solid phase microextraction for terpenes and volatile compounds determination in mastic gum extracts, mastic oil and human urine by GC– MS . Anal. Lett. 45 : 993 – 1003 .
  • Zhang , Z. Y. , M. J. Yang , and J. Pawliszyn . 1994 . Solid-phase microextraction, a solvent-free alternative for sample preparation . Anal. Chem. 17 : 844A – 853A .

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