293
Views
17
CrossRef citations to date
0
Altmetric
Chemometrics

Determination of Pesticide Residues in Fruit and Vegetables by High-Performance Liquid Chromatography–Tandem Mass Spectrometry with Multivariate Response Surface Methodology

, , &
Pages 231-248 | Received 19 Jan 2018, Accepted 27 Mar 2018, Published online: 15 May 2018

References

  • Abdulra’uf, L. B., and G. H. Tan. 2015. Chemometric approach to the optimization of HS-SPME/GC–MS for the determination of multiclass pesticide residues in fruits and vegetables. Food Chem. 177:267–73. doi:10.1016/j.foodchem.2015.01.031.
  • Anastassiades, M., S. J. Lehotay, D. Štajnbaher, and F. J. Schenck. 2003. Fast and easy multiresidue method employing acetonitrile extraction/partitioning and dispersive solid-phase extraction for the determination of pesticide residues in produce. J. AOAC Int. 86 (2):412–31.
  • Aulakh, J., A. Malik, V. Kaur, and P. Schmitt-Kopplin. 2005. A review on solid phase micro extraction-high performance liquid chromatography (SPME-HPLC) analysis of pesticides. Crit. Rev. Anal. Chem. 35 (1):71–85. doi:10.1080/10408340590947952.
  • Chang, C., J. Luo, M. Chen, K. Wu, T. Dong, X. He, K. Zhou, L. Wang, D. Chen, and Z. Zhou. 2016. Determination of twenty organophosphorus pesticides in blood serum by gas chromatography-tandem mass spectrometry. ‎Anal. Methods 8 (22):4487–96. doi:10.1039/c6ay00825a.
  • Cook, J., M. Engel, P. Wylie, and B. Quimby. 1998. Multiresidue screening of pesticides in foods using retention time locking, GC-AED, database search, and GC/MS identification. J. AOAC Int. 82 (2):313–26.
  • Cortada, C., L. Vidal, R. Pastor, N. Santiago, and A. Canals. 2009. Determination of organochlorine pesticides in water samples by dispersive liquid–liquid microextraction coupled to gas chromatography–mass spectrometry. Anal. Chim. Acta 649 (2):218–21. doi:10.1016/j.aca.2009.07.041.
  • Criswell, J. T., K. Shelton, and C. Luper. 2013. Toxicity of pesticides. Pesticide Applicator Certification Series. McAlester, OK, USA: Oklahoma Cooperative Extension Service (EPP-7457).
  • Dong, C.-H., X.-Q. Xie, X.-L. Wang, Y. Zhan, and Y.-J. Yao. 2009. Application of Box–Behnken design in optimisation for polysaccharides extraction from cultured mycelium of Cordyceps sinensis. Food Bioprod. Process. 87 (2):139–44. doi:10.1016/j.fbp.2008.06.004.
  • European Union. 2016. Commission regulation, 2016/486. OJEU 90:1–66.
  • Frenich, A. G., R. Romero-González, and M. Del Mar Aguilera-Luiz. 2014. Comprehensive analysis of toxics (pesticides, veterinary drugs and mycotoxins) in food by UHPLC-MS. Trends Anal. Chem. 63:158–69. doi:10.1016/j.trac.2014.06.020.
  • Gamble, H. 2015. Trends in food production practices relative to foodborne parasites. In Foodborne parasites in the food supply web, 11–22. Cambridge, UK: Woodhead Publishers.
  • Guan, S. H., M. W. Huang, X. Li, and Q. Cai. 2018. Determination of atrazine, simazine, alachlor, and metolachlor in surface water using dispersive pipette extraction and gas chromatography–mass spectrometry. Anal. Lett. 51 (4):613–25. doi:10.1080/00032719.2017.1341904.
  • Gunatilake, S. R., J.-W. Kwon, T. E. Mlsna, and K. Xia. 2014. A novel approach to determine estrogenic hormones in swine lagoon wastewater using the QuEChERS method combined with solid phase extraction and LC/MS/MS analysis. ‎Anal. Methods 6 (23):9267–75. doi:10.1039/c4ay01804d.
  • Jansson, C., T. Pihlström, B.-G. Österdahl, and K. E. Markides. 2004. A new multi-residue method for analysis of pesticide residues in fruit and vegetables using liquid chromatography with tandem mass spectrometric detection. J. Chromatogr. A 1023 (1):93–104. doi:10.1016/j.chroma.2003.10.019.
  • Kaczyński, P. 2017. Large-scale multi-class herbicides analysis in oilseeds by rapid one-step QuEChERS-based extraction and cleanup method using liquid chromatography–tandem mass spectrometry. Food Chem. 230:411–22. doi:10.1016/j.foodchem.2017.03.076.
  • Kittlaus, S., G. Kempe, and T. Glauner. 2011. Multi residue pesticide screening in fruit and vegetables using the G6490A QQQ system, 1–51. Waldbronn, BW Germany: Agilent Technologies.
  • Kruve, A., R. Rebane, K. Kipper, M.-L. Oldekop, H. Evard, K. Herodes, P. Ravio, and I. Leito. 2015. Tutorial review on validation of liquid chromatography–mass spectrometry methods: Part I. Anal. Chim. Acta 870:29–44. doi:10.1016/j.aca.2015.02.017.
  • Lawal, A., G. H. Tan, and A. M. A. Alsharif. 2016. Recent advances in analysis of pesticides in food and drink samples using LPME techniques coupled to GC-MS and LC-MS: A review. J. AOAC Int. 99 (6):1383–94. doi:10.5740/jaoacint.16-0272.
  • Leito, I., K. Herodes, M. Huopolainen, K. Virro, A. Künnapas, A. Kruve, and R. Tanner. 2008. Towards the electrospray ionization mass spectrometry ionization efficiency scale of organic compounds. Rapid Commun. Mass Spectrom. 22 (3):379–84. doi:10.1002/rcm.3371.
  • Li, H., C. Wang, Q. Zhu, H. Du, S. Guan, F. Wang, W. Zhang, W. Fan, Z. Chen, and G. Yang. 2016. Reduction of matrix effects through a simplified QuEChERS method and using small injection volumes in a LC-MS/MS system for the determination of 28 pesticides in fruits and vegetables. ‎Anal. Methods 8 (25):5061–69. doi:10.1039/c6ay00080k.
  • Li, M., C. Dai, F. Wang, Z. Kong, Y. He, Y. T. Huang, and B. Fan. 2017. Chemometric-assisted QuEChERS extraction method for post-harvest pesticide determination in fruits and vegetables. Sci. Rep. 7:42489.
  • Lundanes, E., L. Reubsaet, and T. Greibrokk. 2013. Chromatography: basic principles, sample preparations and related methods. Chichester (UK): John Wiley & Sons.
  • Mostafalou, S., and M. Abdollahi. 2013. Pesticides and human chronic diseases: evidences, mechanisms, and perspectives. Toxicol Appl Pharmacol. 268 (2):157–77. doi:10.1016/j.taap.2013.01.025.
  • Oulkar, D., A. Goon, and K. Banerjee. 2017. Applications of LC-MS/MS in pesticide residue analysis. In Multiresidue methods for the analysis of pesticide residues in food. CRC Press.
  • Parejo, I., O. Jauregui, F. Sánchez-Rabaneda, F. Viladomat, J. Bastida, and C. Codina. 2004. Separation and characterization of phenolic compounds in fennel (Foeniculum vulgare) using liquid chromatography−negative electrospray ionization tandem mass spectrometry. J. Agric. Food Chem. 52 (12):3679–87. doi:10.1021/jf030813h.
  • Parrón, T., M. Requena, A. F. Hernández, and R. Alarcón. 2014. Environmental exposure to pesticides and cancer risk in multiple human organ systems. Toxicol. Lett. 230 (2):157–65. doi:10.1016/j.toxlet.2013.11.009.
  • Rezaee, M., Y. Assadi, M.-R. M. Hosseini, E. Aghaee, F. Ahmadi, and S. Berijani. 2006. Determination of organic compounds in water using dispersive liquid–liquid microextraction. J. Chromatogr. A 1116 (1):1–9. doi:10.1016/j.chroma.2006.03.007.
  • SANTE-11813. 2017. Guidance document on analytical quality control and method validation procedures for pesticide residues and analysis in food and feed. EU: European Commission.
  • Sharma, K. 2013. Mass spectrometry—The early years. Int. J. Mass Spectrom. 349:3–8. doi:10.1016/j.ijms.2013.05.028.
  • Szerkus, O., A. Y. Mpanga, M. J. Markuszewski, R. Kaliszan, and D. Siluk. 2016. Optimization of the electrospray ionization source with the use of the design of experiments approach for the LC–MS-MS determination of selected metabolites in human urine. Highway One South, USA: Pharma/Science Group.
  • Vázquez, P. P., A. Lozano, S. Uclés, M. G. Ramos, and A. Fernández-Alba. 2015. A sensitive and efficient method for routine pesticide multiresidue analysis in bee pollen samples using gas and liquid chromatography coupled to tandem mass spectrometry. J. Chromatogr. A 1426:161–73. doi:10.1016/j.chroma.2015.11.081.
  • Wang, J., Z. Gong, T. Zhang, S. Feng, J. Wang, and Y. Zhang. 2017. Simultaneous determination of 106 pesticides in nuts by LC–MS/MS using freeze‐out combined with dispersive solid‐phase extraction purification. J. Sep. Sci. 40 (11):2398–2405. doi:10.1002/jssc.201700092.
  • Xie, Q., S. Liu, Y. Fan, J. Sun, and X. Zhang. 2014. Determination of phthalate esters in edible oils by use of QuEChERS coupled with ionic-liquid-based dispersive liquid–liquid microextraction before high-performance liquid chromatography. Anal. Bioanal. Chem. 406 (18):4563–69. doi:10.1007/s00216-014-7814-8.
  • Xiu-Ping, Z., M. Lin, H. Lan-Qi, C. Jian-Bo, and Z. Li. 2017. The optimization and establishment of QuEChERS-UPLC-MS/MS method for simultaneously detecting various kinds of pesticides residues in fruits and vegetables. J. Chromatogr. B Analyt. Technol. Biomed. Life Sci. 1060:281. doi:10.1016/j.jchromb.2017.06.008.
  • Zhang, L., F. Chen, S. Liu, B. Chen, and C. Pan. 2012. Ionic liquid‐based vortex‐assisted dispersive liquid–liquid microextraction of organophosphorus pesticides in apple and pear. J. Sep. Sci. 35 (18):2514–19. doi:10.1002/jssc.201101060.
  • Zhu, L., Z. Peng, X. Zhang, J. Yang, X. Lai, and G. Yang. 2017. Determination of polyphenols in Lycium barbarum leaves by high-performance liquid chromatography–tandem mass spectrometry. Anal. Lett. 50 (5):761–76. doi:10.1080/00032719.2016.1202956.

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.