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Chromatography

Simultaneous Determination of Abused Prescription Drugs by Simple Dilute-and-Shoot Gas Chromatography – Flame Ionization Detection (GC-FID)

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Pages 716-728 | Received 18 Mar 2020, Accepted 04 Jun 2020, Published online: 18 Jun 2020

References

  • Abdellatef, H. E., M. M. El-Henawee, H. M. El-Sayed, and M. M. Ayad. 2006. Spectrophotometric and spectrofluorimetric methods for analysis of tramadol, acebutolol and dothiepin in pharmaceutical preparations. Spectrochimica Acta. Part A, Molecular and Biomolecular Spectroscopy 65 (5):1087–92. doi:10.1016/j.saa.2006.02.008.
  • Adamowicz, P., and M. Kała. 2010. Simultaneous screening for and determination of 128 date-rape drugs in urine by gas chromatography-electron ionization-mass spectrometry. Forensic Science International 198 (1–3):39–45. doi:10.1016/j.forsciint.2010.02.012.
  • Burns, J. M., and E. W. Boyer. 2013. Antitussives and substance abuse. Substance Abuse and Rehabilitation 4:75–82. doi:10.2147/SAR.S36761.
  • Cunha, R. R., M. M. A. C. Ribeiro, R. A. A. Muñoz, and E. M. Richter. 2017. Fast determination of codeine, orphenadrine, promethazine, scopolamine, tramadol, and paracetamol in pharmaceutical formulations by capillary electrophoresis. Journal of Separation Science 40 (8):1815–23. doi:10.1002/jssc.201601275.
  • El-Didamony, A. M., and I. I. Ali. 2013. Spectrofluorimetric and spectrophotometric analysis of two analgesic drugs in pharmaceutical formulations and biological fluids. Journal of Forensic Sciences 58 (5):1322–9. doi:10.1111/1556-4029.12170.
  • El-Didamony, A. M., and M. A. Moustafa. 2010. Spectrophotometric determination of diphenhydramine hydrochloride in pharmaceutical preparations and biological fluids via ion-pair formation. Arabian Journal of Chemistry 3 (4):265–70. doi:10.1016/j.arabjc.2010.06.014.
  • El-Sayed, A.-A Y., K. M. Mohamed, A. Y. Nasser, J. Button, and D. W. Holt. 2013. Simultaneous determination of tramadol, O-desmethyltramadol and N-desmethyltramadol in human urine by gas chromatography-mass spectrometry. Journal of Chromatography. B, Analytical Technologies in the Biomedical and Life Sciences 926:9–15. doi:10.1016/j.jchromb.2013.02.019.
  • Eurachem Guide. 2014. The fitness for purpose of analytical methods a laboratory guide to method validation and related topics. Accessed January 15, 2020. https://www.eurachem.org/images/stories/Guides/pdf/MV_guide_2nd_ed_EN.pdf.
  • Fitzgerald, R. L., T. L. Griffin, Y.-M. Yun, R. A. Godfrey, R. West, A. J. Pesce, and D. A. Herold. 2012. Dilute and shoot: Analysis of drugs of abuse using selected reaction monitoring for quantification and full scan product ion spectra for identification. Journal of Analytical Toxicology 36 (2):106–11. doi:10.1093/jat/bkr024.
  • Food and Drug Administration. 2019. Drug abuse and dependence section of labeling for human prescription drug and biological products — content and format. Accessed December 25, 2019. https://www.fda.gov/media/128443/download.
  • Hood, D. J., and H. Y. Cheung. 2003. A chromatographic method for rapid and simultaneous analysis of codeine phosphate, ephedrine HCl and chlorpheniramine maleate in cough-cold syrup formulation. Journal of Pharmaceutical and Biomedical Analysis 30 (5):1595–601. doi:10.1016/j.jchromb.2013.02.019.
  • Huang, M., J. Y. Gao, Z. G. Zhai, Q. L. Liang, Y. M. Wang, Y. Q. Bai, and G. A. Luo. 2012. An HPLC-ESI-MS method for simultaneous determination of fourteen metabolites of promethazine and caffeine and its application to pharmacokinetic study of the combination therapy against motion sickness. Journal of Pharmaceutical and Biomedical Analysis 62:119–28. doi:10.1016/j.jpba.2011.12.033.
  • The International Council for Harmonisation of Technical Requirements for Pharmaceuticals for Human Use. 2005. Validation of analytical procedures: Text and methodology. Accessed January 24, 2020. http://www.gmp-compliance.org/guidemgr/files/Q2(R1).pdf.
  • The International Council for Harmonisation of Technical Requirements for Pharmaceuticals for Human Use. 2019. Bioanalytical method validation M1. Accessed January 5, 2020. https://www.database.ich.org/sites/default/files/M10_EWG_Draft_Guideline.pdf.
  • Kommana, R., and P. Basappa. 2013. Validated stability indicating RP-HPLC method for simultaneous estimation of codeine phosphate and chlorpheniramine maleate from their combined liquid dosage form. Chromatography Research International 2013:1–7. doi:10.1155/2013/404727.
  • Krzek, J., and M. Starek. 2004. Quality assessment for tramadol in pharmaceutical preparations with thin layer chromatography and densitometry. Biomedical Chromatography: BMC 18 (8):589–99. doi:10.1002/bmc.361.
  • Lara, F. J., A. M. García-Campaña, F. Alés-Barrero, and J. M. Bosque-Sendra. 2005. Determination of thiazinamium, promazine and promethazine in pharmaceutical formulations using a CZE method. Analytica Chimica Acta 535 (1–2):101–8. doi:10.1016/j.aca.2004.11.081.
  • Lodha, A., A. Pandya, P. G. Sutariya, and S. K. Menon. 2014. A smart and rapid colorimetric method for the detection of codeine sulphate using unmodified gold nanoprobe. RSC Advances 4 (92):50443–8. doi:10.1039/C4RA06269H.
  • Lynch, K. L., B. J. Shapiro, D. Coffa, S. P. Novak, and A. H. Kral. 2015. Promethazine use among chronic pain patients. Drug and Alcohol Dependence 150:92–7. doi:10.1016/j.drugalcdep.2015.02.023.
  • National Institute on Drug Abuse. 2018. Misuse of prescription drugs. Accessed February 10, 2020. https://www.drugabuse.gov/publications/research-reports/misuse-prescription-drugs.
  • Njuguna, N. M., K. O. Abuga, F. N. Kamau, and G. N. Thoithi. 2017. A liquid chromatography method for simultaneous determination of diphenhydramine, promethazine, chlorpheniramine and ephedrine in cold-cough syrups. Pharmaceutical Chemistry Journal 51 (2):153–8. doi:10.1007/s11094-017-1574-7.
  • NNT. 2012. FDA limits the distribution of certain cough medicines. https://www.pattayamail.com/thailandnews/fda-limits-the-distribution-of-certain-cough-medicines-14468
  • Pereira, P. F., M. C. Marra, R. R. Cunha, W. P. da Silva, R. A. A. Munoz, and E. M. Richter. 2014. Two simple and fast electrochemical methods for simultaneous determination of promethazine and codeine. Journal of Electroanalytical Chemistry 713:32–8. doi:10.1016/j.jelechem.2013.11.031.
  • Post, B. 2016. FDA warns on sales of tramadol to teens. https://www.bangkokpost.com/thailand/general/1166281/fda-warns-on-sales-of-tramadol-to-teens
  • Saif, M. J., and J. Anwar. 2005. A new spectrophotometric method for the determination of promethazine-HCl from pure and pharmaceutical preparations. Talanta 67 (5):869–72. doi:10.1016/j.talanta.2005.03.034.
  • United Nations Office on Drugs and Crime. 2009. Guidance for the validation of analytical methodology and calibration of equipment used for testing of illicit drugs in seized materials and biological specimens. Accessed December 11, 2019. https://www.unodc.org/documents/scientific/validation_E.pdf.
  • Vanhee, C., S. Janvier, G. Moens, E. Deconinck, and P. Courselle. 2016. A simple dilute and shoot methodology for the identification and quantification of illegal insulin. Journal of Pharmaceutical Analysis 6 (5):326–34. doi:10.1016/j.jpha.2016.04.006.

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