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Liquid Chromatography

Rapid Determination of Free Fatty Acids in the Extracellular Medium of Cyanobacteria by Stir Bar Sorptive Extraction (SBSE) Coupled to Ultra-High-Performance Liquid Chromatography – Triple Quadrupole Tandem Mass Spectrometry (UHPLC-MS/MS)

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Pages 2801-2811 | Received 21 Oct 2020, Accepted 14 Feb 2021, Published online: 01 Mar 2021

References

  • Baltussen, E., C. Cramers, and P. Sandra. 2002. Sorptive sample preparation - A review. Analytical and Bioanalytical Chemistry 373 (1-2):3–22. doi:10.1007/s00216-002-1266-2.
  • Baltussen, E., P. Sandra, F. David, and C. Cramers. 1999. Stir bar sorptive extraction (SBSE), a novel extraction technique for aqueous samples: Theory and principles. Journal of Microcolumn Separations 11 (10):737–47. doi:10.1002/(SICI)1520-667X(1999)11:10<737::AID-MCS7>3.0.CO;2-4.
  • Benet, I., C. Ibañez, M. D. Guàrdia, J. Solà, J. Arnau, and E. Roura. 2015. Optimisation of stir-bar sorptive extraction (SBSE), targeting medium and long-chain free fatty acids in cooked ham exudates. Food Chemistry 185:75–83. doi:10.1016/j.foodchem.2015.03.102.
  • Brown, H. A., and R. C. Murphy. 2009. Working towards an exegesis for lipids in biology. Nature Chemical Biology 5 (9):602–6. doi:10.1038/nchembio0909-602.
  • Collin, D. P., P. G. McCormick, and M. G. Schmitt. 1974. Quantitative gas chromatographic determination of short-chain fatty acids in aqueous samples. Clinical Chemistry 20 (9):1235–7.
  • Gao, Z., H. Zhao, Z. Li, X. Tan, and X. Lu. 2012. Photosynthetic production of ethanol from carbon dioxide in genetically engineered cyanobacteria. Energy & Environmental Science 5 (12):9857–65. doi:10.1039/C2EE22675H.
  • Gilart, N., P. A. G. Cormack, R. M. Marce, F. Borrull, and N. Fontanals. 2013. Preparation of a polar monolithic coating for stir bar sorptive extraction of emerging contaminants from wastewaters. Journal of Chromatography A 1295:42–7. doi:10.1016/j.chroma.2013.04.067.
  • Gilart, N., N. Miralles, R. M. Marce, F. Borrull, and N. Fontanals. 2013. Novel coatings for stir bar sorptive extraction to determine pharmaceuticals and personal care products in environmental waters by liquid chromatography and tandem mass spectrometry. Analytica Chimica Acta 774:51–60. doi:10.1016/j.aca.2013.03.010.
  • Guan, W., H. Zhao, X. Lu, C. Wang, M. Yang, and F. Bai. 2011. Quantitative analysis of fatty-acid-based biofuels produced by wild-type and genetically engineered cyanobacteria by gas chromatography-mass spectrometry. Journal of Chromatography A 1218 (45):8289–93. doi:10.1016/j.chroma.2011.09.043.
  • Horák, T., J. Čulík, M. Jurková, P. Čejka, and V. Kellner. 2008. Determination of free medium-chain fatty acids in beer by stir bar sorptive extraction. Journal of Chromatography A 1196:96–9.
  • Kamphorst, J. J., J. Fan, W. Lu, E. White, and J. D. Rabinowitz. 2011. Liquid chromatography-high resolution mass spectrometry analysis of fatty acid metabolism. Analytical Chemistry 83 (23):9114–22. doi:10.1021/ac202220b.
  • Kotani, A., F. Kusu, and K. Takamura. 2002. New electrochemical detection method in high-performance liquid chromatography for determining free fatty acids. Analytica Chimica Acta 465 (1-2):199–206. doi:10.1016/S0003-2670(01)01520-3.
  • Liu, T., and C. Khosla. 2010. Genetic engineering of Escherichia coli for biofuel production. Annual Review of Genetics 44:53–69. doi:10.1146/annurev-genet-102209-163440.
  • Lu, X. 2010. A perspective: Photosynthetic production of fatty acid-based biofuels in genetically engineered cyanobacteria. Biotechnology Advances 28 (6):742–6. doi:10.1016/j.biotechadv.2010.05.021.
  • Margoum, C., C. Guillemain, X. Yang, and M. Coquery. 2013. Stir bar sorptive extraction coupled to liquid chromatography-tandem mass spectrometry for the determination of pesticides in water samples: Method validation and measurement uncertainty. Talanta 116:1–7. doi:10.1016/j.talanta.2013.04.066.
  • Miao, X., and Q. Wu. 2006. Biodiesel production from heterotrophic microalgal oil. Bioresource Technology 97 (6):841–6. doi:10.1016/j.biortech.2005.04.008.
  • Pan, L., M. Adams, and J. Pawliszyn. 1995. Determination of fatty acids using solid phase microextraction. Analytical Chemistry 67 (23):4396–403. doi:10.1021/ac00119a031.
  • Quintana, N., F. Van der Kooy, M. D. Van de Rhee, G. P. Voshol, and R. Verpoorte. 2011. Renewable energy from cyanobacteria: Energy production optimization by metabolic pathway engineering. Applied Microbiology and Biotechnology 91 (3):471–90. doi:10.1007/s00253-011-3394-0.
  • Roberts, L. D., G. Mccombie, C. M. Titman, and J. L. Griffin. 2008. A matter of fat: An introduction to lipidomic profiling methods. Journal of Chromatography. B, Analytical Technologies in the Biomedical and Life Sciences 871 (2):174–81. doi:10.1016/j.jchromb.2008.04.002.
  • Rodil, R., and M. Moeder. 2008. Stir bar sorptive extraction coupled to thermodesorption-gas chromatography-mass spectrometry for the determination of insect repelling substances in water samples. Journal of Chromatography A 1178 (1-2):9–16. doi:10.1016/j.chroma.2007.11.051.
  • Si, Q. Q., F. Li, C. C. Gao, C. Wang, Z. Y. Wang, and J. Zhao. 2016. Detection of phthalate esters in seawater by stir bar sorptive extraction and gas chromatography-mass spectrometry. Marine Pollution Bulletin 108 (1-2):163–70. doi:10.1016/j.marpolbul.2016.04.034.
  • Soini, H. A., K. E. Bruce, D. Wiesler, F. David, P. Sandra, and M. V. Novotny. 2005. Stir bar sorptive extraction: A new quantitative and comprehensive sampling technique for determination of chemical signal profiles from biological media. Journal of Chemical Ecology 31 (2):377–92. doi:10.1007/s10886-005-1347-8.
  • Somerville, C. 2007. Biofuels. Current Biology 17 (4):R115–19. doi:10.1016/j.cub.2007.01.010.
  • Spaepen, M., D. Van Oevelen, and H. Verachtert. 1978. Fatty acids and esters produced during the spontaneous fermentation of lambic and gueuze. Journal of the Institute of Brewing 84 (5):278–82. doi:10.1002/j.2050-0416.1978.tb03888.x.
  • Tan, X., L. Yao, Q. Gao, W. Wang, F. Qi, and X. Lu. 2011. Photosynthesis driven conversion of carbon dioxide to fatty alcohols and hydrocarbons in cyanobacteria. Metabolic Engineering 13 (2):169–76. doi:10.1016/j.ymben.2011.01.001.
  • Tanwar, S., M. D. Carro, and E. Magi. 2015. Innovative sampling and extraction methods for the determination of nonsteroidal anti-inflammatory drugs in water. Journal of Pharmaceutical and Biomedical Analysis 106:100–6. doi:10.1016/j.jpba.2014.10.027.
  • Tomaino, R. M., J. D. Parker, and D. K. Larick. 2001. Analysis of free fatty acids in whey products by solid-phase microextraction. Journal of Agricultural and Food Chemistry 49 (8):3993–8. doi:10.1021/jf001503r.
  • Xu, Q., L. Sheng, B. Li, and Z. Huang. 2011. Determination of free fatty acids in human serum by HPLC-MS. Chemical Analysis and Meterage 20:14–6.

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