160
Views
1
CrossRef citations to date
0
Altmetric
Pharmaceutical Analysis

Response Surface and Freezing-Out Methodologies for the Extraction, Separation, and Validation of Seven Vitamins in a Novel Supplement with Determination by High-Performance Liquid Chromatography

, , , , ORCID Icon &
Pages 1241-1255 | Received 06 Jul 2022, Accepted 12 Sep 2022, Published online: 19 Sep 2022

References

  • Abou-Omar, M., M. Kenawy, A. Youssef, S. Alharthi, M. Attia, and E. Mohamed. 2021. Validation of a novel UPLC-MS/MS method for estimation of metformin and empagliflozin simultaneously in human plasma using freezing lipid precipitation approach and its application to pharmacokinetic study. Journal of Pharmaceutical and Biomedical Analysis 200:114078. doi:10.1016/j.jpba.2021.114078.
  • Bastida, J., M. Gálvez, J. Espín, and A. Sarrías. 2021. Evidence for health properties of pomegranate juices and extracts beyond nutrition: A critical systematic review of human studies. Trends in Food Science and Technology.114:410–23. doi:10.1016/j.tifs.2021.06.014.
  • Bezerra, M. A., R. E. Santelli, E. P. Oliveira, L. S. Villar, and L. A. Escaleira. 2008. Response surface methodology (RSM) as a tool for optimization in analytical chemistry. Talanta 76 (5):965–77. doi:10.1016/j.talanta.2008.05.019.
  • European Medicines Agency (EMEA). ICH Q2 (R1 CPMP/ICH/381/95). Canary Wharf, London, UK. Accessed January 10, 2022. https://www.ema.europa.eu/en/documents/scientific-guideline/ich-q-2-r1-validation-analytical-procedures-text-methodology-step-5_en.pdf.
  • European Union Law (EUR-Lex). Commission Regulation (EC No 1263/96 1996). Accessed January 10, 2022. http://data.europa.eu/eli/reg/1996/1263/oj (EEC) No 2081/92.
  • Feng, L., L. Wu, Y. Guo, N. Hamada, Y. Hashi, X. Li, and L. Cao. 2020. Determination of vitamin D3 in daily oily supplements by a two-dimensional supercritical fluid chromatography-liquid chromatography-mass spectrometry system. Journal of Chromatography A 1629:461510. doi:10.1016/j.chroma.2020.461510.
  • Ferreira, S., R. Bruns, H. S. Ferreira, G. D. Matos, J. M. David, G. C. Brandão, E. da Silva, L. A. Portugal, P. S. dos Reis, A. S. Souza, et al. 2007. Box-Behnken design: An alternative for the optimization of analytical methods. Analytica Chimica Acta 597 (2):179–86. doi:10.1016/j.aca.2007.07.011.
  • Gerster, H. 1997. Vitamin A–functions, dietary requirements and safety in humans. International Journal for Vitamin and Nutrition Research 67 (2):71–90.
  • Gunton, J., C. Girgis, P. Baldock, and P. Lips. 2015. Bone muscle interactions and vitamin D. Bone 80:89–94. doi:10.1016/j.bone.2015.02.029.
  • Karazniewicz-Lada, M., and A. Lowka. 2016. A review of chromatographic methods for the determination of water- and fat-soluble vitamins in biological fluids. Journal of Separation Science.39 (1):132–48. doi:10.05310.1002/jssc.201501038.
  • Karrar, E., I. A. Mohamed Ahmed, T. Huppertz, W. Wei, J. Jin, and X. Wang. 2022. Fatty acid composition and stereospecificity and sterol composition of milk fat from different species. Food Chemistry.128:105313. doi:10.1016/j.idairyj.2021.105313.
  • Kennedy, D. 2016. B vitamins and the brain: Mechanisms, dose and efficacy—A review. Nutrients 8 (2):68. doi:10.3390/nu8020068.
  • Lazzarino, G., S. Longo, A. Amorini, V. D. Pietro, S. D'Urso, G. Lazzarino, A. Belli, and B. Tavazzi. 2017. Single-step preparation of selected biological fluids for the high performance liquid chromatographic analysis of fat-soluble vitamins and antioxidants. Journal of Chromatography. A 1527:43–52. doi:10.1016/j.chroma.2017.10.053.
  • Li, H. B., and F. Chen. 2001. Vitamin B12 in foodstuffs, comparative vitamin B12 assay of foods of animal origin by Lactobacillus leichmannii and Ochromonas malhamensis. Journal of Separation Science.1959 (11):771–4. doi:10.1002/1615-9314(20010401)24.
  • Mandra, V., M. Kouskoura, and C. Markopoulou. 2015. Using the partial least squares method to model the electrospray ionization response produced by small pharmaceutical molecules in positive mode. Rapid Communications in Mass Spectrometry: RCM 29 (18):1661–75. doi:10.1002/rcm.7263.
  • Margaritelis, N., C. Markopoulou, and J. Koundourellis. 2013. Setting up the chromatographic analysis of anthelmintics using the “Crossed D-Optimal” experimental design methodology. Analytical Methods 5 (13):3334. doi:10.1039/c3ay40555a.
  • McMahon, A., H. Mc Nulty, C. Hughes, J. Strain, and M. Ward. 2016. Novel approaches to investigate one-carbon metabolism and related B-vitamins in blood pressure. Nutrients 8 (11):720. doi:10.3390/nu8110720.
  • Melfi, M., D. Nardiello, N. Cicco, V. Candido, and D. Centonze. 2018. Comparative study for the determination of fat-soluble vitamins in rice cereal baby foods using HPLC-DAD and UHPLC-APCI-MS/MS. Foods 10 (3):648. doi:10.3390/foods10030648.
  • Moses, G. 2021. The safety of commonly used vitamins and minerals. Australian Prescriber 44 (4):119–23. doi:10.18773/austprescr.2021.029.
  • NCBI. 2001. https://www.ncbi.nlm.nih.gov/books/NBK56068/table/summarytables.t2/?report=objectonly. Accessed 10 January 2022.
  • Nguyen, T., M. Lee, and G. Lee. 2010. Rapid determination of 95 pesticides in soybean oil using liquid–liquid extraction followed by centrifugation, freezing and dispersive solid phase extraction as cleanup. Microchemical Journal.95 (1):113–9. doi:10.1016/j.microc.2009.11.009.
  • Ostovan, A., M. Ghaedi, M. Arabi, Q. Yang, J. Li, and L. Chen. 2018. Hydrophilic multitemplate molecularly imprinted biopolymers based on a green synthesis strategy for determination of B-family vitamins. ACS Applied Materials & Interfaces 10 (4):4140–50. doi:10.1021/acsami.7b17500.
  • Perales, S., A. Alegria, R. Barbera, and R. Farre. 2005. Review: Determination of vitamin D in dairy products by high performance liquid chromatography. Food Science and Technology International 11 (6):451–62. doi:10.1177/1082013205060129.
  • Rakuša, Z., A. Grobin, and R. Roškar. 2021. A comprehensive approach for the simultaneous analysis of all main water-soluble vitamins in multivitamin preparations by a stability-indicating HPLC-DAD method. Food Chemistry 337:127768. doi:10.1016/j.foodchem.2020.127768.
  • Silva, V. 2018. Utilization of response surface methodology in optimization of extraction of plant materials. In Statistical approaches with emphasis on design of experiments applied to chemical processes, 1st ed. London, UK: Aydar.
  • Temova, Z., and R. Roškar. 2016. Stability-indicating HPLC–UV method for vitamin D3 determination in solutions. Journal of Chromatographic Science 54 (7):1180–6. 10.1093/chromsci/bmw048.
  • Yang, B., X. Li, L. Wang, J. An, T. Wang, F. Zhang, B. Ding, and Y. Li. 2020. A water-stable MOF-AgClO4-abtz as fluorescent sensor for detection of folic acid based on inner filter effect. Talanta 217:121019. doi:10.1016/j.talanta.2020.121019.
  • Zhang, Y., Y. Lin, X. Yang, G. Chen, L. Li, Y. Ma, and J. Liang-Schenkelberg. 2021. Fast determination of vitamin A, vitamin D and vitamin E in food by online SPE combined with heart-cutting two-dimensional liquid chromatography. Journal of Food Composition and Analysis 101:103983. doi:10.1016/j.jfca.2021.103983.
  • Zhao, L., X. Zhao, Y. Xu, X. Liu, J. Zhang, and Z. He. 2021. Simultaneous determination of 49 amino acids, B vitamins, flavonoids, and phenolic acids in commonly consumed vegetables by ultra-performance liquid chromatography-tandem mass spectrometry. Food Chemistry. 344:128712. doi:10.1016/j.foodchem.2020.128712.

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.