Preparation of Porous Silica Particles with a Controlled Mesopore Size by Ultrasonic Spray Drying for High-Performance Liquid Chromatography (HPLC)

References

• Ali, A., F. Ali, and W. J. Cheong. 2017. Sedimentation assisted preparation of ground particles of silica monolith and their C18 modification resulting in a chromatographic phase of improved separation efficiency. Journal of Chromatography A 1525:79–86. doi: 10.1016/j.chroma.2017.10.014.
   PubMedGoogle Scholar
• Baurer, S., S. Polnick, O. L. Sánchez-MunOz, M. Kramer, and M. Lämmerhofer. 2018. N-Propyl-N'-2-pyridylurea-modified silica as mixed-mode stationary phase with moderate weak anion exchange capacity and pH-dependent surface charge reversal. Journal of Chromatography A 1560:45–54. doi: 10.1016/j.chroma.2018.05.012.
   PubMedGoogle Scholar
• Bergna, H. E, and J. J. Kirkland. 1978. Spray dried silica for chromatography. United States Patent 4131542.
   Google Scholar
• Borges, E. M., M. A. Rostagno, and M. Meireles. 2014. Sub-2 μm fully porous and partially porous (core–shell) stationary phases for reversed phase liquid chromatography. RSC Advances 4 (44):22875–87. doi: 10.1039/C3RA45418E.
   Google Scholar
• Deineka, V. I., I. I. Saenko, L. A. Deineka, and I. P. Blinova. 2016. Hydrophilic interaction chromatography as an alternative to reversed-phase HPLC in determining anthocyanins and betacyanins. Journal of Analytical Chemistry 71 (3):297–301. doi: 10.1134/S1061934816030035.
   Google Scholar
• Du, Y. J., L. P. Cheng, L. Chen, Y. C. He, Y. L. Wu, S. S. He, and Y. X. Ke. 2018. Preparation of sub-2 μm large-pore monodispersed mesoporous silica spheres using mixed templates and application in HPLC. Microporous and Mesoporous Materials.265 (15):234–40. doi: 10.1016/j.micromeso.2017.02.051.
   Google Scholar
• Hao, W. Q., B. Di, H. Liu, T. J. Hang, F. Yan, and M. X. Su. 2011. Synthesis and characterization of ordered mesoporous silica spheres using anionic and nonionic mixed surfactants for their potential application in LC. Chromatographia 73 (7-8):623–9. doi: 10.1007/s10337-011-1932-7.
   Google Scholar
• He, C. Y., F. Liu, K. Li, and H. W. Liu. 2006. Molecularly imprinted polymer film grafted from porous silica for selective recognition of testosterone. Analytical Letters 39 (2):275–86. doi: 10.1080/00032710500476946.
   Web of Science ®Google Scholar
• Huo, Z. X., Q. H. Wan, and L. Chen. 2018. Synthesis and evaluation of porous polymethylsilsesquioxane microspheres as low silanol activity chromatographic stationary phase for basic compound separation. Journal of Chromatography. A 1553:90–100. doi: 10.1016/j.chroma.2018.04.024.
   PubMedGoogle Scholar
• Huo, Z. X., Q. H. Wan, and L. Chen. 2020. Energy-efficient and environment-friendly method to prepare monodispersed silica stationary phases for simultaneous separation of compound drugs. Journal of Chromatography A 1618:460866. doi: 10.1016/j.chroma.2020.460866.
   PubMedGoogle Scholar
• Ide, M., E. Wallaert, I. V. Driessche, F. Lynen, P. Sandra, and P. V. D. Voort. 2011. Spherical mesoporous silica particles by spray drying: Doubling the retention factor of HPLC columns. Microporous and Mesoporous Materials 142 (1):282–91. doi: 10.1016/j.micromeso.2010.12.013.
   Google Scholar
• Jiao, J. X., Q. Xu, L. M. Li, T. Tsubasa, and T. Kobayashi. 2008. Effect of PEG with different M/W as template direction reagent on preparation of porous TiO2/SiO2 with assistance of supercritical CO2. Colloid and Polymer Science 286 (13):1485–91. doi: 10.1007/s00396-008-1919-6.
   Google Scholar
• Kirkland, J. J. 1974. Completely porous microspheres for chromatographic uses. United States Patent 3782075.
   Google Scholar
• Kirkland, J. J., F. A. Truszkowski, and R. D. Ricker. 2002. Atypical silica-based column packings for high-performance liquid chromatography. Journal of Chromatography A 965 (1-2):25–34. doi: 10.1016/S0021-9673(01)01339-5.
   PubMedGoogle Scholar
• Peterson, A. K., D. G. Morgan, and S. E. Skrabalak. 2010. Aerosol synthesis of porous particles using simple salts as a pore template. Langmuir: The ACS Journal of Surfaces and Colloids 26 (11):8804–9. doi: 10.1021/la904549t.
   PubMedGoogle Scholar
• Qu, Q. S., H. Xuan, K. H. Zhang, X. M. Chen, S. Y. Sun, Y. Ding, S. J. Feng, and Q. Xu. 2017. Rods-on-sphere silica particles for high performance liquid chromatography. Journal of Chromatography A 1497:87–91. doi: 10.1016/j.chroma.2017.03.051.
   PubMedGoogle Scholar
• Shahnani, M., M. Mohebbi, A. Mehdi, A. Ghassempour, and H. Y. Aboul-Enein. 2018. Silica microspheres from rice husk: A good opportunity for chromatography stationary phase. Industrial Crops and Products 121:236–40. doi: 10.1016/j.indcrop.2018.05.023.
   Google Scholar
• Tanaka, N, and D. V. Mccalley. 2016. Core–shell, ultrasmall particles, monoliths, and other support materials in high-performance liquid chromatography. Analytical Chemistry 88 (1):279–98. doi: 10.1021/acs.analchem.5b04093.
   PubMedGoogle Scholar
• Tanaka, N., H. Nagayama, H. Kobayashi, T. Ikegami, K. Hosoya, N. Ishizuka, H. Minakuchi, K. Nakanishi, K. Cabrera, and D. Lubda. 2000. Monolithic silica columns for HPLC, micro-HPLC, and CEC. Journal of High Resolution Chromatography 23 (1):111–6. doi: 10.1002/(SICI)1521-4168(20000101)23:1<111::AID-JHRC111>3.0.CO;2-H.
   Google Scholar
• Tee, K. H, and L. C. Herng. 2020. Advancements in the preparation and application of monolithic silica columns for efficient separation in liquid chromatography. Talanta 224 (2):121777.
   PubMedGoogle Scholar
• Unger, K. K., R. Skudas, and M. M. Schulte. 2008. Particle packed columns and monolithic columns in high-performance liquid chromatography-comparison and critical appraisal. Journal of Chromatography A 1184 (1-2):393–415. doi: 10.1016/j.chroma.2007.11.118.
   PubMedGoogle Scholar
• Waldron, K., Z. X. Wu, W. Wu, W. J. Liu, D. Y. Zhao, X. D. Chen, and C. Selomulya. 2014. Formation of uniform large SBA-15 microspheres via spray drying. Journal of Materials Chemistry A 2 (45):19500–8. doi: 10.1039/C4TA05002A.
   Google Scholar
• Xia, H. J., J. Wang, G. Chen, J. W. Liu, G. P. Wan, and Q. Bai. 2019. One-pot synthesis of SiO2@SiO2 core-shell microspheres with controllable mesopore size as a new stationary phase for fast HPLC separation of alkylbenzenes and β-agonists. Mikrochimica Acta 186 (2):125–33. doi: 10.1007/s00604-019-3229-8.
   PubMedGoogle Scholar
• Xia, H. J., L. Wang, C. Y. Li, B. Tian, Q. F. Li, H. Zhao, and Q. Bai. 2020. Synthesis of fully porous silica microspheres with high specific surface area for fast HPLC separation of intact proteins and digests of ovalbumin. Mikrochimica Acta 187 (7):382–92. doi: 10.1007/s00604-020-04327-2.
   PubMedGoogle Scholar
• Yang, X. H., G. P. Wan, S. J. Ma, H. J. Xia, J. Wang, J. W. Liu, Y. N. Liu, G. Chen, and Q. Bai. 2020. Synthesis and optimization of SiO2@SiO2 core-shell microspheres by an improved polymerization-induced colloid aggregation method for fast separation of small solutes and proteins. Talanta 207 (15):120310. doi: 10.1016/j.talanta.2019.120310.
   PubMedGoogle Scholar