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Original Articles

Visualization of nanodomain structures in lithium niobate and lithium tantalate crystals by scanning electron microscopy

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Pages 60-67 | Accepted 23 Mar 2016, Published online: 15 Nov 2016

References

  • P. Potnis, N.T. Tsou, J. Huber, A review of domain modelling and domain imaging techniques in ferroelectric crystals, Mater. 4, 417–447 (2011).
  • E. Soergel, Visualization of ferroelectric domains in bulk single crystals, Appl. Phys. B. 81, 729–751 (2005).
  • A. K. Tagantsev, L.E. Cross, J. Fousek, Domains in Ferroic Crystals and Thin Films. Springer; 2010.
  • L. Reimer, Scanning Electron Microscopy, Physics of Image Formation and Microanalysis. Springer; 1998.
  • G. Y. Robinson, R.M. White, Scanning electron microscopy of ferroelectric domains in barium titanate, Appl Phys Lett. 10, 320–322 (1967).
  • R. Le Bihan, C. Sella, Study of domains of ferroelectric crystals with scanning electron microscope, J Phys Soc Jpn. 28, 377–379 (1970).
  • V.Ya. Shur, A.I. Lobov, A.G. Shur, S. Kurimura, Y. Nomura, K. Terabe, X.Y. Liu, K. Kitamura, Rearrangement of ferroelectric domain structure induced by chemical etching, Appl Phys Lett. 87, 022905 (2005).
  • B. Abboud, R. Le Bihan, A. Michelet, F. M'bama, B. Hilczer, Influence of X-ray irradiation of TGS and LATGS on the nucleation of ferroelectric domains with an electron beam and on the activation field, Ferroelectr. 140, 45–51 (1993).
  • N. Nakatani, Ferroelectric domain structure of tri-glycinetriglycine sulfate observed using a scanning electron microscope, Jpn. J. Appl. Phys. 12, 1723–1728 (1973).
  • A. A. Sogr, I.B. Kopylova, The domain contrast and polarization reversal of TGS crystals by scanning electron microscopy in EBIC mode, Ferroelectr. 172, 217–220 (1995).
  • D. S. Chezganov, M.M. Smirnov, D.K. Kuznetsov, V. Ya. Shur, Electron beam domain patterning of MgO-doped lithium niobate crystals covered by resist layer, Ferroelectr. 476, 117–126 (2015).
  • E. V. Emelin, A.I. Il'in, L.S. Kokhanchik, Recording of domains by an electron beam on the surface of +Z cuts of lithium niobate, Phys Sol Stat. 55, 540–546 (2013).
  • L. S. Kokhanchik, M.N. Palatnikov, O.B. Shcherbina, Ferroelectric domains in near-stoichiometric LiNbO3 by e-beam polarization reversal, Phase Trans. 84, 797–803 (2011).
  • V.Ya. Shur, D.S. Chezganov, A.R. Akhmatkhanov, D.K. Kuznetsov, Domain patterning by electron beam of MgO doped lithium niobate covered by resist, Appl Phys Lett. 106, 232902 (2015).
  • V.Ya. Shur, D.S. Chezganov, M.M. Smirnov, D.O. Alikin, M.M. Neradovskiy, D.K. Kuznetsov, Domain switching by electron beam irradiation of Z+-polar surface in Mg-doped lithium niobate, Appl Phys Lett. 105, 052908 (2014).
  • D. Grüner, Z. Shen, Direct scanning electron microscopy imaging of ferroelectric domains after ion milling, J Am Ceram Soc. 93, 48–50 (2010).
  • A. A. Sogr, I.B. Kopylova, Observation of the domain structure of ferroelectrics with the scanning electron microscope, Ferroelectr. 191, 193–198 (1997).
  • R. Le Bihan, Study of ferroelectric and ferroelastic domain structures by scanning electron microscopy, Ferroelectr. 97, 19–46 (1989).
  • R. Le Bihan, M. Maussion, Direct observationof ferro-electric domains in triglycine sulphate (T.G.S.) using the scanning electron microscope (S.E.M.), J Phys Colloq. 33, 217–219 (1972).
  • S. Ikeda, Y. Uchikawa, SEM Imaging of ferroelectric domains, J. Electron Microsc. 29, 209–217 (1980).
  • S. Zhu, W. Cao, Imaging of 180° ferroelectric domains in LiTaO3 by means of scanning electron microscopy, Phys Stat Sol. 173, 2495–2502 (1999).
  • J. Li, H.X. Yang, H.F. Tian, C. Ma, S. Zhang, Y.G. Zhao, J.Q. Li, Scanning secondary-electron microscopy on ferroelectric domains and domain walls in YMnO3, Appl Phys Lett. 100, 152903 (2012).
  • G. Rosenman, A. Skliar, I. Lareah, N. Angert, M. Tseitlin, M. Roth, Observation of ferroelectric domains structures by secondary-electron microscopy in as-grown KTiOPO4 crystals, Phys Rev B. 54, 6222–6226 (1996).
  • K. Tanaka, T. Suhara, Non-destructive observation of ferroelectric domain inverted structures in MgO:LiNbO3 by scanning electron microscope, Electron Lett. 51, 923–925 (2015).
  • G. Rosenman, A. Skliar, Y. Lareah, N. Angert, M. Tseitlin, M. Roth, M. Oron, M. Katz, Asymmetric secondary electron emission flux in ferroelectric KTiOPO4 crystal, J Appl Phys. 80, 7166–7168 (1996).
  • S. Zhu, W. Cao, Imaging of 180° ferroelectric domains in LiTaO3 by means of SEM, Phys Stat Sol (a). 173, 495–502 (1999).
  • A. A. Sogr, Domain structure of ferroelectrics observed in the scanning electron microscope, Ferroelectr. 97, 47–57 (1989).
  • D. J. Stokes, Principles and Practice of Variable Pressure/Environmental Scanning Electron Microscopy (VP-ESEM), John Wiley & Sons, Ltd; 2008.
  • S. Zhu, W. Cao, Direct observation of ferroelectric domains in LiTaO3 using environmental scanning electron microscopy, Phys Rev Lett. 79, 2558–2561 (1997).
  • S. N. Zhu, W. Cao, Imaging of ferroelectric domains in LiTaO3 by environmental scanning electron microscopy, Ferroelectr. 222, 257–262 (1999).
  • W. Cao, Observation of ferroelectric domains using environmental SEM, Microsc Microan. 10, 1072–1073 (2004).
  • J. A. Hooton, W.J. Merz, Etch patterns and ferroelectric domains in BaTiO3 single crystal, Phys Rev. 98, 409–413 (1955).
  • K. Nassau, H.J. Levinstein, G.M. Loiacono, The domain structure and etching of ferroelectric lithium niobate, Appl Phys Lett. 6, 228–229 (1965).
  • X. Liu, K. Terabe, M. Nakamura, S. Takekawa, K. Kitamura, Nanoscale chemical etching of near-stochiometric lithium tantalate, J Appl Phys. 97, 064308 (2005).
  • W. L. Holstein, Etching study of ferroelectric microdomains in LiNbO3 and MgO:LiNbO3, J Cryst Growth. 171, 477–484 (1997).
  • V. Bermúdez, F. Caccavale, C. Sada, F. Segato, Diéguez E, Etching effect on periodic domain structures of lithium niobate crystals, J Cryst Growth. 191, 589–593 (1998).
  • V.Ya. Shur, D. K. Kuznetsov, E.A. Mingaliev, E.M. Yakunina, A.I. Lobov, A.V. Ievlev, In situ investigation of formation of self-assembled nanodomain structure in lithium niobate after pulse laser irradiation, Appl Phys Lett. 99, 082801 (2001).
  • V.Ya. Shur, E.A. Mingaliev, D.K. Kuznetsov, M.S. Kosobokov, Micro- and Nanodomain Structures Produced by Pulse Laser Heating in Congruent Lithium Tantalate, Ferroelectr. 443, 95–102 (2013).
  • V.Ya. Shur, M.S. Kosobokov, E.A. Mingaliev, V.R. Karpov, Formation of the domain structure in CLN under the pyroelectric field induced by pulse infrared laser heating, AIP Advances. 5, 107110 (2015).
  • M. S. Kosobokov, V.Y.A. Shur, E.A. Mingaliev, S.V. Avdoshin, Formation of self-organized nanodomain structures in lithium niobate after pulsed infrared laser heating, Phys Sol Stat. 57, 2020–2024 (2015).

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