An X-Ray Diffraction Study of the Substructure-Superstructure Transformation in α-Bis(1,2-Benzoquinonedioximato)palladium(II), α-Pd(bqd)₂

References

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• Kistenmacher , T. J. and Destro , R. to be published. Details of the X-ray diffraction analyses, including refinements at 295K, 122K, 76K, and 19.5K, will be published elsewhere
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• The 19.5K model was based on rigid α-Pd(bqd)2 molecules with idealized 2/m symmetry and dimensions from our 122K analysis (Ref. 8). The positions and orientations of the molecules were adjusted using conventional difference-Fourier methods; the final R, value (= F,0-F,cF0) was 0.15 for the 1973 reflections with positive net intensity, out of a total of 2625 measured reflections
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