Cross polarization in the tilted frame: assignment and spectral simplification in heteronuclear spin systems

References

• Ernst , R. R. , Bodenhausen , G. and Wokaun , A. 1987 . Principles of Nuclear Magnetic Resonance in One and Two Dimensions Oxford : Clarendon Press .
   Google Scholar
• Wüthrich , K. 1986 . NMR of Proteins and Nucleic Acids New York : Wiley .
   Google Scholar
• Ikura , M. , Kay , L. E. and Bax , A. 1990 . Biochemistry , 29 : 4659
   PubMed Web of Science ®Google Scholar
• Van De Ven , F. J. M. 1995 . Multidimensional NMR in Liquids, Basic Principles and Experimental Methods Weinheim : VCH .
   Google Scholar
• Cavanagh , J. , Fairbrother , W. J. , Palmer , A. G. III and Skelton , N. J. 1996 . Protein NMR Spectroscopy: Principles and Practice San Diego : Academic Press .
   Google Scholar
• Zheng , L. and Herzfeld , J. 1992 . J. Bioenerg. Biomembr. , 24 : 139 Engelhard, M., and Bechinger, B., 1995, Isr. J. Chem. 35, 273; Herzfeld, J., and Hu, J. G., 1996, Encyclopedia of NMR, Vol. 2 (Chichester: Wiley) p. 862; Smith, S. O., Aschheim, K., and Groesbeek, M., 1996, Quart. Rev. Biophys. 29, 395.
   PubMed Web of Science ®Google Scholar
• Griffiths , J. M. , Ashburn , T. T. , Auger , M. , Costa , P. R. , Griffin , R. G. and Lansbury , P. T. 1995 . J. Amer. chem. Soc , 117 : 3539 Lansbury, P. T., Costa, P. R., Griffiths, J. M., Simon, E. J., Auger, M., Halverson, K. J., Kocisko, K. J., Hendsch, Z. S., Ashburn, T. T., Spencer, R. G. S., Tidor, B., and Griffin, R. G., 1995, Nat. Struct. Biol. 2, 990.
   Web of Science ®Google Scholar
• Hirsh , D. J. , Hammer , J. , Maloy , W. L. , Blazyk , J. and Schaefer , J. 1996 . Biochemistry , 35 : 12 – 733 .
   Web of Science ®Google Scholar
• Heller , J. , Larsen , A. C. , Ernst , M. , Bekker , T. , Baldwin , M. , Prusiner , S. B. , Pines , A. and Wemmer , D. E. 1996 . Protein Sci. , 5 : 1655
   PubMed Web of Science ®Google Scholar
• Andrew , E. R. , Bradbury , A. and Eades , R. G. 1958 . Nature , 182 : 1659 Lowe, I. J., 1959, Phys. Rev. Lett. 2, 285; Andrew, E. R., Bradbury, A., and Eades, R. G., 1959, Nature 183, 1802.
   Web of Science ®Google Scholar
• Opella , S. J. and Waugh , J. S. 1977 . J. chem. Phys. , 66 : 4919 see, e.g. Sanders, C. K., Hare, B. J., Howard, K. P., and Prestegard, J. H., 1994, Progr. nucl. magn. Res. Spectrosc. 26, 421; Tjandra, N., and Bax, A., 1997, Science 278, 1111.
   Web of Science ®Google Scholar
• Bennett , A. E. , Griffin , R. G. and Vega , S. 1994 . Recoupling of Homo- and Heteronuclear Dipolar Interactions in Rotating Solids Berlin : Springer Verlag . For recent comparative studies, see, e.g. Baldus, M., Geurts, D. G., and Meier, B. H., 1998, Solid State NMR 11, 157.
   Google Scholar
• Schaefer , J. , Stejskal , E. G. , Garbow , J. R. and Kay , R. A. 1984 . J. magn. Reson. , 59 : 150
   Web of Science ®Google Scholar
• Gullion , T. and Schaefer , J. 1989 . J. magn. Reson. , 81 : 196 Hing, A. W., Vega, S., and Schaefer, J., 1992, J. magn. Reson. 96, 205.
   Web of Science ®Google Scholar
• Sun , B. Q. , Costa , P. R. and Griffin , R. G. 1995 . J. magn. Reson. A , 112 : 191
   Google Scholar
• Baldus , M. , Geurts , D. G. , Hediger , S. and Meier , B. H. 1996 . J. magn. Reson. A , 118 : 140
   Google Scholar
• Baldus , M. , Iuliucci , R. J. and Meier , B. H. 1997 . J. Amer. chem. Soc , 119 : 1121
   Web of Science ®Google Scholar
• Hartmann , S. R. and Hahn , E. L. 1962 . Phys. Rev. , 128 : 2042
   Web of Science ®Google Scholar
• Pines , A. , Gibby , M. G. and Waugh , J. S. 1973 . J. chem. Phys. , 59 : 569
   Web of Science ®Google Scholar
• Hediger , S. , Meier , B. H. , Kurur , N. D. , Bodenhausen , G. and Ernst , R. R. 1994 . Chem. Phys. Lett. , 223 : 283 Hediger, S., Meier, B. H., and Ernst, R. R., 1995, Chem. Phys. Lett. 240, 449.
   Web of Science ®Google Scholar
• Strauss , S. K. , Bremi , T. and Ernst , R. R. 1998 . J. biomol. NMR , 12 : 39
   PubMed Web of Science ®Google Scholar
• Caravatti , P. , Bodenhausen , G. and Ernst , R. R. 1983 . J. magn. Reson. , 55 : 88
   Web of Science ®Google Scholar
• Meier , B. H. 1994 . Adv. magn. opt. Reson. , 18 : 1
   Google Scholar
• Lee , M. and Goldburg , W. I. 1965 . Phys. Rev. A , 140 : 1261
   Web of Science ®Google Scholar
• Wu , C. H. , Ramamoorthy , A. and Opella , S. J. 1994 . J. magn. Reson. A , 109 : 270
   Google Scholar
• Baldus , M. and Meier , B. H. 1997 . J. magn. Reson. , 128 : 172
   Web of Science ®Google Scholar
• Takegoshi , K. , Nomura , K. and Terao , T. 1995 . Chem. Phys. Lett. , 232 : 424 1997, J. magn. Reson. 127, 206.
   Web of Science ®Google Scholar
• Costa , P. R. , Sun , B. Q. and Griffin , R. G. 1997 . J. Amer. chem. Soc , 119 : 10821
   Web of Science ®Google Scholar
• Mehring , M. 1983 . Principles of High Resolution NMR in Solids Berlin : Springer Verlag .
   Google Scholar
• Oas , T. G. , Griffin , R. G. and Levitt , M. H. 1988 . J. chem. Phys. , 89 : 692 Levitt, M. H., Oas, T. G., and Griffin, R. G., 1988, Isr. J. Chem. 28, 271.
   Web of Science ®Google Scholar
• Costa , P. R. , Gross , J. D. , Hong , M. and Griffin , R. G. 1997 . Chem. Phys. Lett. , 280 : 95
   Web of Science ®Google Scholar
• Gan , Z. H. and Grant , D. M. 1990 . Chem. Phys. Lett. , 168 : 304
   Web of Science ®Google Scholar
• Stejskal , E. O. , Schaefer , J. and Waugh , J. S. 1977 . J. magn. Reson. , 28 : 105
   Web of Science ®Google Scholar
• Sardashti , M. and Maciel , G. E. 1987 . J. magn. Reson. , 72 : 467
   Web of Science ®Google Scholar
• Wind , R. A. , Dec , S. F. , Lock , H. and Maciel , G. E. 1988 . J. magn. Reson. , 79 : 136
   Web of Science ®Google Scholar
• Meier , B. H. 1992 . Chem. Phys. Lett. , 188 : 201
   Web of Science ®Google Scholar
• Andrew , E. R. , Bradbury , A. , Eades , R. G. and Wynn , V. T. 1963 . Phys. Lett. , 4 : 99
   Web of Science ®Google Scholar
• Raleigh , D. P. , Levitt , M. H. and Griffin , R. G. 1988 . Chem. Phys. Lett. , 146 : 71 Levitt, M. H., Raleigh, D. P., and Griffin, R. G., 1990, J. chem. Phys. 92, 6347.
   Web of Science ®Google Scholar
• Colombo , M. G. , Meier , B. H. and Ernst , R. R. 1988 . Chem. Phys. Lett. , 146 : 189
   Web of Science ®Google Scholar
• Smith , S. A. , Levante , T. O. , Meier , B. H. and Ernst , R. R. 1994 . J. magn. Reson. A , 106 : 75
   Google Scholar
• Ye , C. , Fu , R. , Hu , J. , Hou , L. and Ding , S. 1993 . Magn. Res. Chem. , 31 : 699 Oas, T. G., Hartzell, C. J., Dahlquist, F. W., and Drobny, G. P., 1987, J. Amer. chem. Soc 109, 5962.
   Web of Science ®Google Scholar
• Abragam , A. 1961 . The Principles of Nuclear Magnetism Oxford : Clarendon Press .
   Google Scholar
• Verel , R. , Baldus , M. , Nijman , M. , van Os , J. and Meier , B. H. 1997 . Chem. Phys. Lett. , 280 : 31
   Web of Science ®Google Scholar
• Verel , R. , Baldus , M. , Ernst , M. and Meier , B. H. 1998 . Chem. Phys. Lett. , 287 : 421
   Web of Science ®Google Scholar
• Greenstein , J. P. and Winitz , M. 1961 . Chemistry of the Amino Acids New York : Wiley .
   Google Scholar
• Bennett , A. E. , Rienstra , C. M. , Auger , M. , Lakshmi , K. V. and Griffin , R. G. 1995 . J. chem. Phys. , 103 : 1
   Web of Science ®Google Scholar
• Rienstra , C. M. , Gamburg , A. , Gross , J. D. , Hu , J. G. , Itin , B. A. , Rovnyak , D. S. and Griffin , R. G. 1998 . J. magn. Reson. , to be published.
   Google Scholar
• Verhoeven , A. , Verel , R. and Meier , B. H. 1997 . Chem. Phys. Lett. , 266 : 465
   Web of Science ®Google Scholar
• Petkova , A. T. , Baldus , M. , Hong , M. , Herzfeld , J. and Griffin , R. G. unpublished.
   Google Scholar
• Maudsley , A. A. and Ernst , R. R. 1977 . Chem. Phys. Lett. , 50 : 368 This work was presented in part at the 39th ENC, Asilomar, CA in 1998.
   Web of Science ®Google Scholar